5-cyclohexyloxy-1-[N'-(9H-fluoren-9-ylidene)]-3-oxopyrazolidine-1-ium-2-ide

Base Information

Chemical Name:5-cyclohexyloxy-1-[N'-(9H-fluoren-9-ylidene)]-3-oxopyrazolidine-1-ium-2-ide
CAS No.:1401072-51-2
Molecular Formula:C₂₂H₂₂N₂O₂
Molecular Weight:346.429
Hs Code.:

Synonyms:5-cyclohexyloxy-1-[N'-(9H-fluoren-9-ylidene)]-3-oxopyrazolidine-1-ium-2-ide

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Chemical Property of 5-cyclohexyloxy-1-[N'-(9H-fluoren-9-ylidene)]-3-oxopyrazolidine-1-ium-2-ide

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Technology Process of 5-cyclohexyloxy-1-[N'-(9H-fluoren-9-ylidene)]-3-oxopyrazolidine-1-ium-2-ide

There total 3 articles about 5-cyclohexyloxy-1-[N'-(9H-fluoren-9-ylidene)]-3-oxopyrazolidine-1-ium-2-ide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1401072-51-2
5-cyclohexyloxy-1-[N'-(9H-fluoren-9-ylidene)]-3-oxopyrazolidine-1-ium-2-ide

Guidance literature:: at 150 ℃; for 3h; Inert atmosphere; Microwave irradiation;

Reference yield: 68.0%

: 2182-55-0
vinyl cyclohexyl ether

: 1401072-73-8
phenyl 2-(9H-fluoren-9-ylidene)hydrazine-1-carboxylate

: 1401072-51-2
5-cyclohexyloxy-1-[N'-(9H-fluoren-9-ylidene)]-3-oxopyrazolidine-1-ium-2-ide

Guidance literature:: at 100 ℃; for 2h; Inert atmosphere;
DOI:10.1021/acs.joc.6b02713

Reference yield:

: 486-25-9,952573-42-1
9-fluorenone

: 1401072-51-2
5-cyclohexyloxy-1-[N'-(9H-fluoren-9-ylidene)]-3-oxopyrazolidine-1-ium-2-ide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid / methanol / Reflux

2: 2 h / 100 °C / Microwave irradiation; Sealed tube

With acetic acid; In methanol;
DOI:10.1021/ja305491t