Technology Process of TK4547-070E
There total 5 articles about TK4547-070E which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
In
ethanol;
at 60 ℃;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: thionyl chloride / N,N-dimethyl-formamide / chloroform / 3 h / Inert atmosphere; Reflux
2.1: ammonium hydroxide / acetonitrile / 0.5 h / 0 °C
3.1: sodium hydroxide / dimethyl sulfoxide / 0.25 h / 10 °C
3.2: 0.58 h
4.1: ethanol / 60 °C
With
ammonium hydroxide; thionyl chloride; sodium hydroxide;
N,N-dimethyl-formamide;
In
ethanol; chloroform; dimethyl sulfoxide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: N,N,N,N,-tetramethylethylenediamine; n-butyllithium / tetrahydrofuran; hexanes / 1 h / -78 °C / Inert atmosphere
1.2: 0.33 h
1.3: pH 1 / Acidic aqueous solution
2.1: nitric acid; sulfuric acid / 1.18 h / 90 °C
3.1: thionyl chloride / N,N-dimethyl-formamide / chloroform / 3 h / Inert atmosphere; Reflux
4.1: ammonium hydroxide / acetonitrile / 0.5 h / 0 °C
5.1: sodium hydroxide / dimethyl sulfoxide / 0.25 h / 10 °C
5.2: 0.58 h
6.1: ethanol / 60 °C
With
ammonium hydroxide; n-butyllithium; thionyl chloride; N,N,N,N,-tetramethylethylenediamine; sulfuric acid; nitric acid; sodium hydroxide;
N,N-dimethyl-formamide;
In
tetrahydrofuran; hexanes; ethanol; chloroform; dimethyl sulfoxide; acetonitrile;
![1-[N-methyl-N-(phenyl)aminocarbonylmethyl]piperazine](/Databaselist/images/loading.webp)
