2-(6-amino-3-methyl-1-(10H-phenothiazin-2-yl)-4,5-dihydro-1H-pyrazolo[3,4-d]pyrimidin-4-yl)phenol

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Chemical Name:2-(6-amino-3-methyl-1-(10H-phenothiazin-2-yl)-4,5-dihydro-1H-pyrazolo[3,4-d]pyrimidin-4-yl)phenol
CAS No.:1580464-35-2
Molecular Formula:C₂₄H₂₀N₆OS
Molecular Weight:440.528
Hs Code.:

Synonyms:2-(6-amino-3-methyl-1-(10H-phenothiazin-2-yl)-4,5-dihydro-1H-pyrazolo[3,4-d]pyrimidin-4-yl)phenol

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Chemical Property of 2-(6-amino-3-methyl-1-(10H-phenothiazin-2-yl)-4,5-dihydro-1H-pyrazolo[3,4-d]pyrimidin-4-yl)phenol

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Technology Process of 2-(6-amino-3-methyl-1-(10H-phenothiazin-2-yl)-4,5-dihydro-1H-pyrazolo[3,4-d]pyrimidin-4-yl)phenol

There total 3 articles about 2-(6-amino-3-methyl-1-(10H-phenothiazin-2-yl)-4,5-dihydro-1H-pyrazolo[3,4-d]pyrimidin-4-yl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1072135-11-5
3-methyl-1-(10H-phenothiazin-8-yl)-1H-pyrazol-5-(4H)-one

: 90-02-8
salicylaldehyde

: 1580464-35-2
2-(6-amino-3-methyl-1-(10H-phenothiazin-2-yl)-4,5-dihydro-1H-pyrazolo[3,4-d]pyrimidin-4-yl)phenol

Guidance literature:: With phosphorus pentoxide; guanidine hydrochloride; In ethanol; for 5h; Reflux;
DOI:10.1016/j.bmcl.2014.02.012

Reference yield:

: 7643-08-5
2-(methylthio)-10H-phenothiazine

: 1580464-35-2
2-(6-amino-3-methyl-1-(10H-phenothiazin-2-yl)-4,5-dihydro-1H-pyrazolo[3,4-d]pyrimidin-4-yl)phenol

Guidance literature:: Multi-step reaction with 3 steps

1: hydrazine / Reflux

2: sodium ethanolate / Reflux

3: guanidine hydrochloride; phosphorus pentoxide / ethanol / 5 h / Reflux

With phosphorus pentoxide; guanidine hydrochloride; sodium ethanolate; hydrazine; In ethanol;
DOI:10.1016/j.bmcl.2014.02.012

Reference yield:

: 1072135-10-4
1-(10H-phenothiazin-8-yl)hydrazine

: 1580464-35-2
2-(6-amino-3-methyl-1-(10H-phenothiazin-2-yl)-4,5-dihydro-1H-pyrazolo[3,4-d]pyrimidin-4-yl)phenol

Guidance literature:: Multi-step reaction with 2 steps

1: sodium ethanolate / Reflux

2: guanidine hydrochloride; phosphorus pentoxide / ethanol / 5 h / Reflux

With phosphorus pentoxide; guanidine hydrochloride; sodium ethanolate; In ethanol;
DOI:10.1016/j.bmcl.2014.02.012