(3aR,4S,6aR)-4-(Benzyloxy-fluoro-methyl)-4-fluoro-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole

Base Information

Chemical Name:(3aR,4S,6aR)-4-(Benzyloxy-fluoro-methyl)-4-fluoro-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole
CAS No.:372955-05-0
Molecular Formula:C₁₅H₁₈F₂O₄
Molecular Weight:300.302
Hs Code.:

Synonyms:(3aR,4S,6aR)-4-(Benzyloxy-fluoro-methyl)-4-fluoro-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole

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Chemical Property of (3aR,4S,6aR)-4-(Benzyloxy-fluoro-methyl)-4-fluoro-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole

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Technology Process of (3aR,4S,6aR)-4-(Benzyloxy-fluoro-methyl)-4-fluoro-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole

There total 1 articles about (3aR,4S,6aR)-4-(Benzyloxy-fluoro-methyl)-4-fluoro-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 28070-06-6
benzyl-3,4-O-isopropylidene-β-D-erythro-pentoribopyranosid-2-ulose

: 372955-05-0
(3aR,4S,6aR)-4-(Benzyloxy-fluoro-methyl)-4-fluoro-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole

Guidance literature:: With 4,4'-diaminostilbene-2,2'-disulfonic acid; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1016/S0040-4020(01)00620-2

Reference yield: 70.0%

: 100-51-6,185532-71-2
benzyl alcohol

: 372955-05-0
(3aR,4S,6aR)-4-(Benzyloxy-fluoro-methyl)-4-fluoro-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole

: C₂₂H₂₄O₅

Guidance literature:: With bis(cyclopentadienyl)hafnium dichloride; 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; at -50 - 20 ℃; for 1.5h;
DOI:10.1016/S0040-4020(01)00620-2

Reference yield: 66.0%

: 100-51-6,185532-71-2
benzyl alcohol

: 372955-05-0
(3aR,4S,6aR)-4-(Benzyloxy-fluoro-methyl)-4-fluoro-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole

: (3aR,4S,6aR)-4-Benzyloxy-4-(bis-benzyloxy-methyl)-2,2-dimethyl-tetrahydro-furo[3,4-d][1,3]dioxole

Guidance literature:: With bis(cyclopentadienyl)hafnium dichloride; 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; at -50 - 20 ℃; for 3h;
DOI:10.1016/S0040-4020(01)00620-2