dibenzyl <<<3-methyl-4-phenyl>oxy>carbonyl>-L-glutamate

Base Information

Chemical Name:dibenzyl <<<3-methyl-4-phenyl>oxy>carbonyl>-L-glutamate
CAS No.:156078-83-0
Molecular Formula:C₃₁H₃₄Cl₂N₂O₆
Molecular Weight:601.527
Hs Code.:

dibenzyl <<<3-methyl-4-<bis(2-chloroethyl)amino>phenyl>oxy>carbonyl>-L-glutamate

Synonyms:dibenzyl <<<3-methyl-4-phenyl>oxy>carbonyl>-L-glutamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dibenzyl <<<3-methyl-4-phenyl>oxy>carbonyl>-L-glutamate

Chemical Property:

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Technology Process of dibenzyl <<<3-methyl-4-phenyl>oxy>carbonyl>-L-glutamate

There total 6 articles about dibenzyl <<<3-methyl-4-phenyl>oxy>carbonyl>-L-glutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 2791-84-6,227205-81-4
L-glutamic acid dibenzyl ester 4-toluenesulfonate

: 156079-36-6
4'-nitrophenyl 4-phenyl carbonate

: 156078-83-0
dibenzyl <<<3-methyl-4-phenyl>oxy>carbonyl>-L-glutamate

Guidance literature:: With triethylamine; In chloroform; at 50 ℃; for 5h;
DOI:10.1021/jm00026a013

Reference yield:

: 2835-99-6
4-amino-3-methylphenol

: 156078-83-0
dibenzyl <<<3-methyl-4-phenyl>oxy>carbonyl>-L-glutamate

Guidance literature:: Multi-step reaction with 6 steps

1: 30 percent / aq. AcOH / 48 h / Ambient temperature

2: 84 percent / KOH / ethanol / 2 h / Heating

3: 84 percent / CH₃SO₂Cl, pyridine / 0.25 h / 70 °C

4: 57 percent / H₂, HCl / 30percent Pd/C / ethanol; diethyl ether

5: 67 percent / Et₃N / CHCl₃ / 12 h / Ambient temperature

6: 50 percent / Et₃N / CHCl₃ / 5 h / 50 °C

With pyridine; hydrogenchloride; potassium hydroxide; hydrogen; acetic acid; methanesulfonyl chloride; triethylamine; palladium on activated charcoal; In diethyl ether; ethanol; chloroform;
DOI:10.1021/jm00026a013

Reference yield:

: 156079-08-2
3-methyl-4-phenol

: 156078-83-0
dibenzyl <<<3-methyl-4-phenyl>oxy>carbonyl>-L-glutamate

Guidance literature:: Multi-step reaction with 5 steps

1: 84 percent / KOH / ethanol / 2 h / Heating

2: 84 percent / CH₃SO₂Cl, pyridine / 0.25 h / 70 °C

3: 57 percent / H₂, HCl / 30percent Pd/C / ethanol; diethyl ether

4: 67 percent / Et₃N / CHCl₃ / 12 h / Ambient temperature

5: 50 percent / Et₃N / CHCl₃ / 5 h / 50 °C

With pyridine; hydrogenchloride; potassium hydroxide; hydrogen; methanesulfonyl chloride; triethylamine; palladium on activated charcoal; In diethyl ether; ethanol; chloroform;
DOI:10.1021/jm00026a013