Technology Process of C24H30Cl2N3O12P
There total 18 articles about C24H30Cl2N3O12P which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-Bromosuccinimide;
In
water; acetonitrile;
at -5 ℃;
for 0.05h;
DOI:10.1021/ja411733s
- Guidance literature:
-
With
N-Bromosuccinimide; water;
In
acetonitrile;
at -5 ℃;
for 0.05h;
Overall yield = 56 %; Overall yield = 10.5 mg;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: selectfluor / acetonitrile / 25 °C
2.1: tetrabutyl ammonium fluoride / acetonitrile / 2 h / 0 - 25 °C
3.1: 5-(ethylthio)-1H-tetrazole / acetonitrile / 2 h / 25 °C / Inert atmosphere
3.2: 0.5 h / Inert atmosphere
4.1: hydrazine / tetrahydrofuran; water / 0.08 h / 25 °C
5.1: acetic acid / dimethyl sulfoxide / 5 h / 37 °C
6.1: N-Bromosuccinimide / acetonitrile; water / 0.05 h / -5 °C
With
N-Bromosuccinimide; selectfluor; tetrabutyl ammonium fluoride; acetic acid; 5-(ethylthio)-1H-tetrazole; hydrazine;
In
tetrahydrofuran; water; dimethyl sulfoxide; acetonitrile;
DOI:10.1021/ja411733s