Technology Process of C51H86O11Si4
There total 6 articles about C51H86O11Si4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C48H84O10Si4;
With
lithium hexamethyldisilazane;
In
tetrahydrofuran;
at 0 ℃;
acryloyl chloride;
In
tetrahydrofuran;
at 0 ℃;
DOI:10.1021/jm061071x
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: 55 percent / Red-Al / tetrahydrofuran / 0 °C
2.1: lithium hexamethyldisilazide / tetrahydrofuran / 0 °C
2.2: 43 percent / tetrahydrofuran / 0 °C
With
sodium bis(2-methoxyethoxy)aluminium dihydride; lithium hexamethyldisilazane;
In
tetrahydrofuran;
DOI:10.1021/jm061071x
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: Red-Al / tetrahydrofuran / 0 °C
2.1: imidazole
3.1: diethyl ether / 0 °C
4.1: imidazole
5.1: 55 percent / Red-Al / tetrahydrofuran / 0 °C
6.1: lithium hexamethyldisilazide / tetrahydrofuran / 0 °C
6.2: 43 percent / tetrahydrofuran / 0 °C
With
1H-imidazole; sodium bis(2-methoxyethoxy)aluminium dihydride; lithium hexamethyldisilazane;
In
tetrahydrofuran; diethyl ether;
DOI:10.1021/jm061071x