((1R,5S)-2-methyl-1-(3-phenylprop-2-ynyl)-5-(prop-1-en-2-yl)cyclohex-2-enyloxy)-triethylsilane

Base Information

• Chemical Name: ((1R,5S)-2-methyl-1-(3-phenylprop-2-ynyl)-5-(prop-1-en-2-yl)cyclohex-2-enyloxy)-triethylsilane
• CAS No.: 937369-20-5
• Molecular Formula: C₂₅H₃₆OSi
• Molecular Weight: 380.646

Synonyms:((1R,5S)-2-methyl-1-(3-phenylprop-2-ynyl)-5-(prop-1-en-2-yl)cyclohex-2-enyloxy)-triethylsilane

Chemical Property of ((1R,5S)-2-methyl-1-(3-phenylprop-2-ynyl)-5-(prop-1-en-2-yl)cyclohex-2-enyloxy)-triethylsilane

Chemical Property:

Purity/Quality:

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Technology Process of ((1R,5S)-2-methyl-1-(3-phenylprop-2-ynyl)-5-(prop-1-en-2-yl)cyclohex-2-enyloxy)-triethylsilane

There total 1 articles about ((1R,5S)-2-methyl-1-(3-phenylprop-2-ynyl)-5-(prop-1-en-2-yl)cyclohex-2-enyloxy)-triethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

iodobenzene (591-50-4) + C19H32OSi → ((1R,5S)-2-methyl-1-(3-phenylprop-2-ynyl)-5-(prop-1-en-2-yl)cyclohex-2-enyloxy)-triethylsilane (937369-20-5)

Guidance literature:

iodobenzene; With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; Inert atmosphere;

C₁₉H₃₂OSi; With triethylamine; Inert atmosphere;

DOI:10.1016/j.tet.2008.11.103

Reference yield: 67.0%

((1R,5S)-2-methyl-1-(3-phenylprop-2-ynyl)-5-(prop-1-en-2-yl)cyclohex-2-enyloxy)-triethylsilane (937369-20-5) → (3aS,6S,7aR)-3a-methyl-1-phenyl-6-(prop-1-en-2-yl)-3,3a,5,6,7,7a-hexahydroinden-4-one

Guidance literature:

With silver hexafluoroantimonate; (triphenylphosphine)gold(I) chloride; In dichloromethane; isopropyl alcohol; at 23 ℃; for 0.166667h;

DOI:10.1002/anie.200604544

upstream raw materials:

iodobenzene

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