(E)-P,P-diphenyl-N-[3,4-dihydronaphthalen-1(2H)-ylidene]phosphinic amide

Base Information

Chemical Name:(E)-P,P-diphenyl-N-[3,4-dihydronaphthalen-1(2H)-ylidene]phosphinic amide
CAS No.:154051-01-1
Molecular Formula:C₂₂H₂₀NOP
Molecular Weight:345.381
Hs Code.:

Synonyms:(E)-P,P-diphenyl-N-[3,4-dihydronaphthalen-1(2H)-ylidene]phosphinic amide

Suppliers and Price of (E)-P,P-diphenyl-N-[3,4-dihydronaphthalen-1(2H)-ylidene]phosphinic amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-P,P-diphenyl-N-[3,4-dihydronaphthalen-1(2H)-ylidene]phosphinic amide

Chemical Property:

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Technology Process of (E)-P,P-diphenyl-N-[3,4-dihydronaphthalen-1(2H)-ylidene]phosphinic amide

There total 3 articles about (E)-P,P-diphenyl-N-[3,4-dihydronaphthalen-1(2H)-ylidene]phosphinic amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3349-64-2,68253-36-1,100485-58-3
1-tetralone oxime

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 154051-01-1
(E)-P,P-diphenyl-N-[3,4-dihydronaphthalen-1(2H)-ylidene]phosphinic amide

Guidance literature:: With triethylamine; In dichloromethane; Petroleum ether; at -45 ℃; for 0.5h;
DOI:10.1002/chem.200900210

Reference yield:

: 529-34-0
3,4-dihydronaphthalene-1(2H)-one

: 154051-01-1
(E)-P,P-diphenyl-N-[3,4-dihydronaphthalen-1(2H)-ylidene]phosphinic amide

Guidance literature:: Multi-step reaction with 2 steps

1: hydroxylamine hydrochloride; sodium acetate / methanol / Inert atmosphere

2: triethylamine / hexane; dichloromethane / Inert atmosphere

With hydroxylamine hydrochloride; sodium acetate; triethylamine; In methanol; hexane; dichloromethane;
DOI:10.1021/ol302079q

Reference yield:

: 5994-87-6
diphenylphosphinamide

: 529-34-0
3,4-dihydronaphthalene-1(2H)-one

: 154051-01-1
(E)-P,P-diphenyl-N-[3,4-dihydronaphthalen-1(2H)-ylidene]phosphinic amide

Guidance literature:: With titanium(IV) tetraethanolate; In toluene; at 120 ℃; for 24h; Glovebox; Inert atmosphere;
DOI:10.1002/anie.201809930