N³-(benzyloxycarbonyl)-L-(2,3-diaminopropanoyl)-L-alanine trifluoroacetate salt

Base Information

Chemical Name:N³-(benzyloxycarbonyl)-L-(2,3-diaminopropanoyl)-L-alanine trifluoroacetate salt
CAS No.:122593-32-2
Molecular Formula:C₂HF₃O₂*C₁₄H₁₉N₃O₅
Molecular Weight:423.346
Hs Code.:

N<sup>3</sup>-(benzyloxycarbonyl)-L-(2,3-diaminopropanoyl)-L-alanine trifluoroacetate salt

Synonyms:N³-(benzyloxycarbonyl)-L-(2,3-diaminopropanoyl)-L-alanine trifluoroacetate salt

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Chemical Property of N³-(benzyloxycarbonyl)-L-(2,3-diaminopropanoyl)-L-alanine trifluoroacetate salt

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Technology Process of N³-(benzyloxycarbonyl)-L-(2,3-diaminopropanoyl)-L-alanine trifluoroacetate salt

There total 2 articles about N³-(benzyloxycarbonyl)-L-(2,3-diaminopropanoyl)-L-alanine trifluoroacetate salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 122593-28-6
N²-(tert-butoxycarbonyl)-N³-(benzyloxycarbonyl)-L-(2,3-diaminopropanoyl)-L-alanine tert-butyl ester

: 76-05-1
trifluoroacetic acid

: 122593-32-2
N³-(benzyloxycarbonyl)-L-(2,3-diaminopropanoyl)-L-alanine trifluoroacetate salt

Guidance literature:: for 2h; Ambient temperature;
DOI:10.1021/jm00163a022

Reference yield:

: 65710-57-8,81306-93-6
N²-(tert-butoxycarbonyl)-N³-(benzyloxycarbonyl)-L-2,3-diaminopropanoic acid

: 122593-32-2
N³-(benzyloxycarbonyl)-L-(2,3-diaminopropanoyl)-L-alanine trifluoroacetate salt

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / DPPA, Et₃N / dimethylformamide / 12 h / Ambient temperature

2: 82 percent / 2 h / Ambient temperature

With diphenyl-phosphinic acid; triethylamine; In N,N-dimethyl-formamide;
DOI:10.1021/jm00163a022