benzyl (2S,3R)-3-((tert-butoxycarbonyl)amino)-2-((diphenylmethylene)amino)-3-phenylpropanoate

Base Information

Chemical Name:benzyl (2S,3R)-3-((tert-butoxycarbonyl)amino)-2-((diphenylmethylene)amino)-3-phenylpropanoate
CAS No.:1431529-34-8
Molecular Formula:C₃₄H₃₄N₂O₄
Molecular Weight:534.655
Hs Code.:

Synonyms:benzyl (2S,3R)-3-((tert-butoxycarbonyl)amino)-2-((diphenylmethylene)amino)-3-phenylpropanoate

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Chemical Property of benzyl (2S,3R)-3-((tert-butoxycarbonyl)amino)-2-((diphenylmethylene)amino)-3-phenylpropanoate

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Technology Process of benzyl (2S,3R)-3-((tert-butoxycarbonyl)amino)-2-((diphenylmethylene)amino)-3-phenylpropanoate

There total 2 articles about benzyl (2S,3R)-3-((tert-butoxycarbonyl)amino)-2-((diphenylmethylene)amino)-3-phenylpropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 81477-91-0
benzyl 2-(diphenylmethyleneamino)acetate

: 150884-50-7
benzaldehyde N-boc imine

: 1431529-34-8
benzyl (2S,3R)-3-((tert-butoxycarbonyl)amino)-2-((diphenylmethylene)amino)-3-phenylpropanoate

Guidance literature:: With (S)-2-(2,3-bis(dicyclohexylamino)cyclopropenimine)-3-phenylpropan-1-ol; In toluene; at 20 ℃; for 0.166667h; Molecular sieve;

Reference yield:

: 81477-91-0
benzyl 2-(diphenylmethyleneamino)acetate

: 150884-50-7
benzaldehyde N-boc imine

: 1431529-34-8
benzyl (2S,3R)-3-((tert-butoxycarbonyl)amino)-2-((diphenylmethylene)amino)-3-phenylpropanoate

: benzyl (2R,3S)-3-((tert-butoxycarbonyl)amino)-2-((diphenylmethylene)amino)-3-phenylpropanoate

: benzyl 3-((tert-butoxycarbonyl)amino)-2-((diphenylmethylene)amino)-3-phenylpropanoate

Guidance literature:: With (R)-3-(benzyloxy)-2-(3-(3,5-bis(trifluoromethyl)phenyl)ureido)-N,N-dimethyl-N-(naphthalen-1-ylmethyl)-3,3-diphenylpropan-1-aminium bromide; caesium carbonate; In toluene; at 20 ℃; for 24h; Overall yield = 89 percent; stereoselective reaction;
DOI:10.1016/j.tet.2020.131484