C₂₃H₃₀ClN₅O₅S

Base Information

Chemical Name:C₂₃H₃₀ClN₅O₅S
CAS No.:1159610-50-0
Molecular Formula:C₂₃H₃₀ClN₅O₅S
Molecular Weight:524.041
Hs Code.:

C<sub>23</sub>H<sub>30</sub>ClN<sub>5</sub>O<sub>5</sub>S

Synonyms:C₂₃H₃₀ClN₅O₅S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₃₀ClN₅O₅S

Chemical Property:

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Technology Process of C₂₃H₃₀ClN₅O₅S

There total 11 articles about C₂₃H₃₀ClN₅O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₂₈ClN₅O₅S

: 1159610-50-0
C₂₃H₃₀ClN₅O₅S

Guidance literature:: With methanol; sodium tetrahydroborate; acetic acid; In tetrahydrofuran; at 0 - 50 ℃; pH=5;

Reference yield:

: 18437-63-3
tert-butyl N-(4-nitrophenyl)carbamate

: 1159610-50-0
C₂₃H₃₀ClN₅O₅S

Guidance literature:: Multi-step reaction with 9 steps

1.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 16 h

2.1: isopropyl alcohol / 16 h / Reflux

3.1: dmap / tetrahydrofuran / 16 h / Reflux

4.1: hydrazine / ethanol / 3 h / Reflux

5.1: dmap; diisopropyl-carbodiimide / chloroform / 0 - 20 °C

6.1: dichloromethane; 1,4-dioxane / 1 h / 20 °C

7.1: sodium cyanoborohydride / N,N-dimethyl-formamide; methanol / 16 h / 20 °C

8.1: sodium nitrate / water; acetic acid / 0.5 h / 0 °C

8.2: 5 h / 0 °C

9.1: water; methanol / 1 h / 20 °C

9.2: 0 - 50 °C / pH 5

With dmap; sodium nitrate; hydrogen; sodium cyanoborohydride; hydrazine; diisopropyl-carbodiimide; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; chloroform; water; acetic acid; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 100-01-6,104810-17-5
4-nitro-aniline

: 1159610-50-0
C₂₃H₃₀ClN₅O₅S

Guidance literature:: Multi-step reaction with 11 steps

1.1: dmap / acetonitrile / 16 h / Reflux

2.1: potassium carbonate / methanol / 16 h / Reflux

3.1: hydrogen / palladium 10% on activated carbon / ethyl acetate / 16 h

4.1: isopropyl alcohol / 16 h / Reflux

5.1: dmap / tetrahydrofuran / 16 h / Reflux

6.1: hydrazine / ethanol / 3 h / Reflux

7.1: dmap; diisopropyl-carbodiimide / chloroform / 0 - 20 °C

8.1: dichloromethane; 1,4-dioxane / 1 h / 20 °C

9.1: sodium cyanoborohydride / N,N-dimethyl-formamide; methanol / 16 h / 20 °C

10.1: sodium nitrate / water; acetic acid / 0.5 h / 0 °C

10.2: 5 h / 0 °C

11.1: water; methanol / 1 h / 20 °C

11.2: 0 - 50 °C / pH 5

With dmap; sodium nitrate; hydrogen; sodium cyanoborohydride; potassium carbonate; hydrazine; diisopropyl-carbodiimide; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; dichloromethane; chloroform; water; acetic acid; ethyl acetate; N,N-dimethyl-formamide; isopropyl alcohol; acetonitrile;