N-Benzyl-3-oxa-7-azabicyclo<3.3.1>nonane Perchlorate

Base Information

Chemical Name:N-Benzyl-3-oxa-7-azabicyclo<3.3.1>nonane Perchlorate
CAS No.:77716-10-0
Molecular Formula:C₁₄H₁₉NO*ClHO₄
Molecular Weight:317.769
Hs Code.:

Synonyms:N-Benzyl-3-oxa-7-azabicyclo<3.3.1>nonane Perchlorate

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Chemical Property of N-Benzyl-3-oxa-7-azabicyclo<3.3.1>nonane Perchlorate

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Technology Process of N-Benzyl-3-oxa-7-azabicyclo<3.3.1>nonane Perchlorate

There total 4 articles about N-Benzyl-3-oxa-7-azabicyclo<3.3.1>nonane Perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.2%

: 77716-06-4
N-Benzyl-3-oxa-7-azabicyclo<3.3.1>nonane

: 77716-10-0
N-Benzyl-3-oxa-7-azabicyclo<3.3.1>nonane Perchlorate

Guidance literature:: In diethyl ether; at 0 ℃; for 0.5h;
DOI:10.1021/jo00329a010

Reference yield:

: 29943-42-8,143562-54-3
Tetrahydro-4H-pyran-4-one

: 77716-10-0
N-Benzyl-3-oxa-7-azabicyclo<3.3.1>nonane Perchlorate

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / methanol / 6 h / Heating

2: 1.) 85percent aq. Hydrazine hydrate, 2.) 85percent aq. KOH / 1.) Triethylene glycol, 60 deg C, 2.) 145 deg C, 4h

3: 99.2 percent / diethyl ether / 0.5 h / 0 °C

With potassium hydroxide; hydrazine hydrate; In methanol; diethyl ether;
DOI:10.1021/jo00329a010

Reference yield:

: 2182-52-7
benzylamine acetic acid

: 77716-10-0
N-Benzyl-3-oxa-7-azabicyclo<3.3.1>nonane Perchlorate

Guidance literature:: Multi-step reaction with 3 steps

1: 72 percent / methanol / 6 h / Heating

2: 1.) 85percent aq. Hydrazine hydrate, 2.) 85percent aq. KOH / 1.) Triethylene glycol, 60 deg C, 2.) 145 deg C, 4h

3: 99.2 percent / diethyl ether / 0.5 h / 0 °C

With potassium hydroxide; hydrazine hydrate; In methanol; diethyl ether;
DOI:10.1021/jo00329a010