C₂₆H₃₄O₉

Base Information

Chemical Name:C₂₆H₃₄O₉
CAS No.:1362110-39-1
Molecular Formula:C₂₆H₃₄O₉
Molecular Weight:490.551
Hs Code.:

C<sub>26</sub>H<sub>34</sub>O<sub>9</sub>

Synonyms:C₂₆H₃₄O₉

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Chemical Property of C₂₆H₃₄O₉

Chemical Property:

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Technology Process of C₂₆H₃₄O₉

There total 17 articles about C₂₆H₃₄O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₆H₃₄O₈

: 1362110-39-1
C₂₆H₃₄O₉

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In water; tert-butyl alcohol; at 20 ℃; for 24h;
DOI:10.1021/ol300390k

Reference yield:

: 1362110-27-7
C₃₂H₄₆O₃Si

: 1362110-39-1
C₂₆H₃₄O₉

Guidance literature:: Multi-step reaction with 14 steps

1.1: dichloromethane / 0.33 h / 0 °C / Inert atmosphere

2.1: sodium hydroxide / methanol; water / 0.33 h / 20 °C

3.1: N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

4.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

5.2: brine

6.1: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

7.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

8.1: sodium cyanoborohydride / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 24 h / 66 °C / Inert atmosphere

9.1: ammonia / methanol; water / 6 h / 66 °C

9.2: 0 °C / pH 2

10.1: pyridine / acetonitrile / 0.5 h / 0 °C / Inert atmosphere

11.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / 100 °C / Inert atmosphere

12.1: N-ethyl-N,N-diisopropylamine; sodium iodide / 1,2-dimethoxyethane / 24 h / Reflux

13.1: ozone / 1,1-dichloroethane / -95 °C

13.2: -95 - 20 °C

14.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 24 h / 20 °C

With pyridine; 1H-imidazole; tert.-butylhydroperoxide; sodium chlorite; sodium dihydrogenphosphate; N-chloro-succinimide; 2-methyl-but-2-ene; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; bis(acetylacetonate)oxovanadium; 2,2'-azobis(isobutyronitrile); tetrabutyl ammonium fluoride; tetrabutyl-ammonium chloride; ammonia; iodine; tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium cyanoborohydride; sodium hydrogencarbonate; potassium carbonate; ozone; N-ethyl-N,N-diisopropylamine; triphenylphosphine; sodium iodide; sodium hydroxide; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; 1,2-dimethoxyethane; 1,1-dichloroethane; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; tert-butyl alcohol; 6.1: Sharpless epoxidation / 14.1: Kraus oxidation;
DOI:10.1021/ol300390k

Reference yield:

: C₃₉H₅₁ClO₆Si

: 1362110-39-1
C₂₆H₃₄O₉

Guidance literature:: Multi-step reaction with 13 steps

1.1: sodium hydroxide / methanol; water / 0.33 h / 20 °C

2.1: N-chloro-succinimide; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; tetrabutyl-ammonium chloride; sodium hydrogencarbonate; potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

3.1: tetra-(n-butyl)ammonium iodide; sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide / 0.17 h / 0 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

4.2: brine

5.1: tert.-butylhydroperoxide; bis(acetylacetonate)oxovanadium / dichloromethane / 2 h / 20 °C / Inert atmosphere; Molecular sieve

6.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

7.1: sodium cyanoborohydride / tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide / 24 h / 66 °C / Inert atmosphere

8.1: ammonia / methanol; water / 6 h / 66 °C

8.2: 0 °C / pH 2

9.1: pyridine / acetonitrile / 0.5 h / 0 °C / Inert atmosphere

10.1: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / 100 °C / Inert atmosphere

11.1: N-ethyl-N,N-diisopropylamine; sodium iodide / 1,2-dimethoxyethane / 24 h / Reflux

12.1: ozone / 1,1-dichloroethane / -95 °C

12.2: -95 - 20 °C

13.1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene / water; tert-butyl alcohol / 24 h / 20 °C

With pyridine; 1H-imidazole; tert.-butylhydroperoxide; sodium chlorite; sodium dihydrogenphosphate; N-chloro-succinimide; 2-methyl-but-2-ene; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; bis(acetylacetonate)oxovanadium; 2,2'-azobis(isobutyronitrile); tetrabutyl ammonium fluoride; tetrabutyl-ammonium chloride; ammonia; iodine; tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium cyanoborohydride; sodium hydrogencarbonate; potassium carbonate; ozone; N-ethyl-N,N-diisopropylamine; triphenylphosphine; sodium iodide; sodium hydroxide; In tetrahydrofuran; methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; 1,2-dimethoxyethane; 1,1-dichloroethane; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; tert-butyl alcohol; 5.1: Sharpless epoxidation / 13.1: Kraus oxidation;
DOI:10.1021/ol300390k