1,3-bis(2,6-diisopropylphenyl)-2-trimethylsilylimidazolium triflate

Base Information

• Chemical Name: 1,3-bis(2,6-diisopropylphenyl)-2-trimethylsilylimidazolium triflate
• CAS No.: 1228185-14-5
• Molecular Formula: CF₃O₃S*C₃₀H₄₅N₂Si
• Molecular Weight: 610.857

Synonyms:1,3-bis(2,6-diisopropylphenyl)-2-trimethylsilylimidazolium triflate

Chemical Property of 1,3-bis(2,6-diisopropylphenyl)-2-trimethylsilylimidazolium triflate

Chemical Property:

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Technology Process of 1,3-bis(2,6-diisopropylphenyl)-2-trimethylsilylimidazolium triflate

There total 1 articles about 1,3-bis(2,6-diisopropylphenyl)-2-trimethylsilylimidazolium triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

trimethylsilyl trifluoromethanesulfonate (27607-77-8) + 1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene (244187-81-3) → 1,3-bis(2,6-diisopropylphenyl)-2-trimethylsilylimidazolium triflate (1228185-14-5)

Guidance literature:

In fluorobenzene; at 0 ℃; for 1h; Inert atmosphere;

DOI:10.1021/om4002268

Reference yield: 90.0%

1,3-bis(2,6-diisopropylphenyl)-2-trimethylsilylimidazolium triflate (1228185-14-5) → C27H36AsCl2N2(1+)*CF3O3S(1-)

Guidance literature:

With arsenic trichloride; In fluorobenzene; at 20 ℃; for 20h; Inert atmosphere;

DOI:10.1021/acs.inorgchem.5b00765

Reference yield: 35.0%

1,3-bis(2,6-diisopropylphenyl)-2-trimethylsilylimidazolium triflate (1228185-14-5) → 1,3-bis(2,6-diisopropylphenyl)-4-trimethylsilylimidazol-2-ylidene (1228185-20-3)

Guidance literature:

With potassium hexamethylsilazane; In tetrahydrofuran; at -78 ℃; Inert atmosphere;

DOI:10.1021/ja102639a

upstream raw materials:

trimethylsilyl trifluoromethanesulfonate

1,3-bis-(2,6-diisopropylphenyl)-imidazol-2-ylidene

Downstream raw materials:

1,3-bis(2,6-diisopropylphenyl)-4-trimethylsilylimidazol-2-ylidene

(P(C₃H₂N₂(C₆H₃(C₃H₇)2)2))2

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