Technology Process of C17H20N2O5
There total 4 articles about C17H20N2O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine;
In
isopropyl alcohol;
at 20 ℃;
for 18h;
Inert atmosphere;
DOI:10.1002/chem.201200457
- Guidance literature:
-
Multi-step reaction with 2 steps
1: dichloromethane / 2 h / 20 °C / Inert atmosphere
2: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 18 h / 20 °C / Inert atmosphere
With
N-ethyl-N,N-diisopropylamine;
In
dichloromethane; isopropyl alcohol;
DOI:10.1002/chem.201200457
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 6 h / 0 - 20 °C / Inert atmosphere
2: dichloromethane / 2 h / 20 °C / Inert atmosphere
3: N-ethyl-N,N-diisopropylamine / isopropyl alcohol / 18 h / 20 °C / Inert atmosphere
With
dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; isopropyl alcohol;
DOI:10.1002/chem.201200457