Norcamphor, dehydro-

Base Information

• Chemical Name: Norcamphor, dehydro-
• CAS No.: 694-98-4
• Molecular Formula: C7H8O
• Molecular Weight: 108.14
• Hs Code.: 2914299000
• Mol file: 694-98-4.mol

Synonyms:5-Norbornen-2-one(6CI,7CI,8CI);(?à)-Bicyclo[2.2.1]hept-5-en-2-one;(?à)-Norborn-5-en-2-one;2-Norbornen-5-one;2-Norbornenone;2-Oxo-5-norbornene;Dehydronorcamphor;NSC152327;Norcamphor, dehydro-;

Chemical Property of Norcamphor, dehydro-

Chemical Property:

• Vapor Pressure: 0.824mmHg at 25°C
• Refractive Index: 1.545
• Boiling Point: 182.1 °C at 760 mmHg
• Flash Point: 63.5 °C
• PSA: 17.07000
• Density: 1.138 g/cm³
• LogP: 1.15150

Purity/Quality:

98% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Norcamphor, dehydro-

There total 43 articles about Norcamphor, dehydro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2-chlorobicyclo<2.2.1>hept-5-ene-2-carbonitrile (6945-87-5) → norborn-5-en-2-one (694-98-4)

Guidance literature:

With potassium hydroxide; In water; dimethyl sulfoxide; for 48h; Ambient temperature;

DOI:10.1021/ja00384a038

Reference yield: 90.0%

5-norbornene-2-ol (694-97-3) → norborn-5-en-2-one (694-98-4)

Guidance literature:

With dipyridinium dichromate; pyridinium trifluroacetate; In dichloromethane; for 6h; Ambient temperature;

DOI:10.1021/jo01311a047

Reference yield: 84.0%

exo-5-norbornen-2-ol (2890-98-4,13080-90-5,16620-80-7,69769-90-0,71030-14-3,71030-15-4,87392-59-4,106928-44-3,694-97-3) → norborn-5-en-2-one (694-98-4)

Guidance literature:

With chromium trioxide-pyridine complex; In dichloromethane; for 2h; Ambient temperature;

DOI:10.1002/hlca.19800630409

upstream raw materials:

endo-5-norbornen-2-ol

1-Chlortetracyclo<3.2.0.0^2,7.0^4,6>heptan

2-chlorobicyclo<2.2.1>hept-5-ene-2-carbonitrile

5-norbornene-2-ol

Downstream raw materials:

3-phenyl-3,3a,4,6,7,7a-hexahydro-4,7-methano-benzotriazol-5-one

2-methylbicyclo<2.2.1>hept-5-en-2endo-ol

endo-2-vinylbicyclo<2.2.1>hept-5-en-2-ol

4-norborn-5-en-2-yl-morpholine