[(E)-4-Methylstyryl]hexyl ketone

Base Information

Chemical Name:[(E)-4-Methylstyryl]hexyl ketone
CAS No.:74975-52-3
Molecular Formula:C16H22 O
Molecular Weight:230.3453
Hs Code.:
NSC Number:326120
DSSTox Substance ID:DTXSID90422954
Nikkaji Number:J3.028.633B
Wikidata:Q82235041

Synonyms:NSC326120;74975-52-3;SCHEMBL11946437;DTXSID90422954;[(E)-4-Methylstyryl]hexyl ketone;NSC-326120

Suppliers and Price of [(E)-4-Methylstyryl]hexyl ketone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of [(E)-4-Methylstyryl]hexyl ketone

Chemical Property:

Vapor Pressure:2.72E-05mmHg at 25°C
Boiling Point:357.5°Cat760mmHg
Flash Point:135.4°C
Density:0.948g/cm³
XLogP3:4.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:7
Exact Mass:230.167065321
Heavy Atom Count:17
Complexity:234

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCCCCC(=O)C=CC1=CC=C(C=C1)C
Isomeric SMILES:CCCCCCC(=O)/C=C/C1=CC=C(C=C1)C

Technology Process of [(E)-4-Methylstyryl]hexyl ketone

There total 5 articles about [(E)-4-Methylstyryl]hexyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 115085-25-1
1-(4-methylphenyl)-non-2-yn-1-ol

: 1357265-95-2
(Z)-1-(4-methylphenyl)-1-nonen-3-one

: 74975-52-3
(E)-1-(4-methylphenyl)-1-nonen-3-one

Guidance literature:: With silver 12-molybdophosphate; In acetone; at 20 ℃; for 1h; optical yield given as %de; stereoselective reaction;
DOI:10.1002/anie.201106381

Reference yield: 85.0%

: 115085-25-1
1-(4-methylphenyl)-non-2-yn-1-ol

: 74975-52-3
(E)-1-(4-methylphenyl)-1-nonen-3-one

Guidance literature:: With molybdophosphoric acid hydrate; In ethyl acetate; at 20 ℃; for 72h; optical yield given as %de; stereoselective reaction;
DOI:10.1002/anie.201106381

Reference yield:

: 629-05-0
n-octyne

: 74975-52-3
(E)-1-(4-methylphenyl)-1-nonen-3-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: ethylmagnesium bromide / tetrahydrofuran; diethyl ether / 1 h / -78 °C

1.2: -78 - 20 °C

1.3: 20 °C

2.1: molybdophosphoric acid hydrate / ethyl acetate / 72 h / 20 °C

With molybdophosphoric acid hydrate; ethylmagnesium bromide; In tetrahydrofuran; diethyl ether; ethyl acetate; 2.1: Meyer-Schuster rearrangement;
DOI:10.1002/anie.201106381