Technology Process of C42H28N2O2
There total 4 articles about C42H28N2O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine;
In
tetrahydrofuran;
at 60 ℃;
for 8h;
Inert atmosphere;
DOI:10.1021/jo201594u
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium carbonate / N,N-dimethyl-formamide / 18 h / Inert atmosphere; Reflux
2: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / tetrahydrofuran / 8 h / 60 °C / Inert atmosphere
With
copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); potassium carbonate; triethylamine;
In
tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jo201594u
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tert.-butylhydroperoxide; bromine / nitrobenzene / 1 h / 110 °C / Inert atmosphere; Irradiation
2: sodium dithionite / tetrahydrofuran; water / 6 h / 20 °C / Inert atmosphere
3: potassium carbonate / N,N-dimethyl-formamide / 18 h / Inert atmosphere; Reflux
4: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / tetrahydrofuran / 8 h / 60 °C / Inert atmosphere
With
tert.-butylhydroperoxide; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); sodium dithionite; bromine; potassium carbonate; triethylamine;
In
tetrahydrofuran; water; nitrobenzene; N,N-dimethyl-formamide;
DOI:10.1021/jo201594u
