1D-3,6-di-O-benzyl-4,5-di-O-(but-2-enyl)-1-O-p-methoxybenzyl-myo-inositol

Base Information

Chemical Name:1D-3,6-di-O-benzyl-4,5-di-O-(but-2-enyl)-1-O-p-methoxybenzyl-myo-inositol
CAS No.:162879-76-7
Molecular Formula:C₃₆H₄₄O₇
Molecular Weight:588.741
Hs Code.:

Synonyms:1D-3,6-di-O-benzyl-4,5-di-O-(but-2-enyl)-1-O-p-methoxybenzyl-myo-inositol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1D-3,6-di-O-benzyl-4,5-di-O-(but-2-enyl)-1-O-p-methoxybenzyl-myo-inositol

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Technology Process of 1D-3,6-di-O-benzyl-4,5-di-O-(but-2-enyl)-1-O-p-methoxybenzyl-myo-inositol

There total 3 articles about 1D-3,6-di-O-benzyl-4,5-di-O-(but-2-enyl)-1-O-p-methoxybenzyl-myo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 824-94-2
p-methoxybenzyl chloride

: 162991-40-4
1D-3,6-di-O-benzyl-4,5-di-O-(but-2-enyl)-myo-inositol

: 162879-76-7
1D-3,6-di-O-benzyl-4,5-di-O-(but-2-enyl)-1-O-p-methoxybenzyl-myo-inositol

Guidance literature:: With tetrabutylammomium bromide; di(n-butyl)tin oxide; In acetonitrile; for 7h; Heating;
DOI:10.1016/0008-6215(94)84005-9

Reference yield:

: 117307-15-0,173828-64-3
D-(+)-3,6-di-O-benzyl-1,2-O-isopropylidene-myo-inositol

: 162879-76-7
1D-3,6-di-O-benzyl-4,5-di-O-(but-2-enyl)-1-O-p-methoxybenzyl-myo-inositol

Guidance literature:: Multi-step reaction with 3 steps

1: NaH / dimethylformamide

2: HCl / methanol / 0.5 h / Heating

3: 82 percent / dibutyltin oxide, tetrabutylammonium bromide / acetonitrile / 7 h / Heating

With hydrogenchloride; tetrabutylammomium bromide; sodium hydride; di(n-butyl)tin oxide; In methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/0008-6215(94)84005-9

Reference yield:

: 162991-39-1
(3aR,4R,5S,6S,7R,7aS)-4,7-Bis-benzyloxy-5,6-bis-[((E)-but-2-enyl)oxy]-2,2-dimethyl-hexahydro-benzo[1,3]dioxole

: 162879-76-7
1D-3,6-di-O-benzyl-4,5-di-O-(but-2-enyl)-1-O-p-methoxybenzyl-myo-inositol

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / methanol / 0.5 h / Heating

2: 82 percent / dibutyltin oxide, tetrabutylammonium bromide / acetonitrile / 7 h / Heating

With hydrogenchloride; tetrabutylammomium bromide; di(n-butyl)tin oxide; In methanol; acetonitrile;
DOI:10.1016/0008-6215(94)84005-9