4-(dimethylamino)-2,6-bis<-N-<3-<(2-nitrophenyl)dithio>propyl>amino>methyl>pyridine

Base Information

• Chemical Name: 4-(dimethylamino)-2,6-bis<-N-<3-<(2-nitrophenyl)dithio>propyl>amino>methyl>pyridine
• CAS No.: 173318-27-9
• Molecular Formula: C₃₉H₄₀N₈O₈S₆
• Molecular Weight: 941.191
• Mol file: 173318-27-9.mol

Synonyms:4-(dimethylamino)-2,6-bis<-N-<3-<(2-nitrophenyl)dithio>propyl>amino>methyl>pyridine

Chemical Property of 4-(dimethylamino)-2,6-bis<-N-<3-<(2-nitrophenyl)dithio>propyl>amino>methyl>pyridine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-(dimethylamino)-2,6-bis<-N-<3-<(2-nitrophenyl)dithio>propyl>amino>methyl>pyridine

There total 2 articles about 4-(dimethylamino)-2,6-bis<-N-<3-<(2-nitrophenyl)dithio>propyl>amino>methyl>pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

2-nitrobenzenesulfenyl chloride (7669-54-7) + {2,6-Bis-[(3-tert-butylsulfanyl-propylamino)-methyl]-pyridin-4-yl}-dimethyl-amine (173318-22-4) → 4-(dimethylamino)-2,6-bis<-N-<3-<(2-nitrophenyl)dithio>propyl>amino>methyl>pyridine (173318-27-9)

Guidance literature:

With acetic acid; for 16h; Ambient temperature;

DOI:10.1021/jm950831t

Reference yield:

4-(dimethylamino)pyridine-2,6-dicarbaldehyde (153504-00-8) → 4-(dimethylamino)-2,6-bis<-N-<3-<(2-nitrophenyl)dithio>propyl>amino>methyl>pyridine (173318-27-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 39 percent / sodium cyanoborohydride / methanol / 36 h / Ambient temperature

2: 61 percent / acetic acid / 16 h / Ambient temperature

With sodium cyanoborohydride; acetic acid; In methanol;

DOI:10.1021/jm950831t

Reference yield: 90.0%

4-(dimethylamino)-2,6-bis<-N-<3-<(2-nitrophenyl)dithio>propyl>amino>methyl>pyridine (173318-27-9) → 4-(dimethylamino)-2,6-bis<propyl>amino>methyl>pyridine (173318-29-1)

Guidance literature:

With hydrogenchloride; 3-Methylindole; In methanol; dichloromethane; for 9h; Ambient temperature;

DOI:10.1021/jm950831t

upstream raw materials:

2-nitrobenzenesulfenyl chloride

{2,6-Bis-[(3-tert-butylsulfanyl-propylamino)-methyl]-pyridin-4-yl}-dimethyl-amine

4-(dimethylamino)pyridine-2,6-dicarbaldehyde

Downstream raw materials:

4-(dimethylamino)-2,6-bis<propyl>amino>methyl>pyridine