Hexadecanoic acid (S)-2-[12-(2,2,2-trichloro-1,1-dimethyl-ethoxycarbonylamino)-dodecanoyloxy]-3-trityloxy-propyl ester

Base Information

Chemical Name:Hexadecanoic acid (S)-2-[12-(2,2,2-trichloro-1,1-dimethyl-ethoxycarbonylamino)-dodecanoyloxy]-3-trityloxy-propyl ester
CAS No.:250142-16-6
Molecular Formula:C₅₅H₈₀Cl₃NO₇
Molecular Weight:973.602
Hs Code.:

Synonyms:Hexadecanoic acid (S)-2-[12-(2,2,2-trichloro-1,1-dimethyl-ethoxycarbonylamino)-dodecanoyloxy]-3-trityloxy-propyl ester

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Chemical Property of Hexadecanoic acid (S)-2-[12-(2,2,2-trichloro-1,1-dimethyl-ethoxycarbonylamino)-dodecanoyloxy]-3-trityloxy-propyl ester

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Technology Process of Hexadecanoic acid (S)-2-[12-(2,2,2-trichloro-1,1-dimethyl-ethoxycarbonylamino)-dodecanoyloxy]-3-trityloxy-propyl ester

There total 4 articles about Hexadecanoic acid (S)-2-[12-(2,2,2-trichloro-1,1-dimethyl-ethoxycarbonylamino)-dodecanoyloxy]-3-trityloxy-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.5%

: 32899-42-6
1-palmitoyl-3-triphenylmethyl-sn-glycerol

: 12-(2,2,2-trichloro-1,1-dimethyl-ethoxycarbonylamino)-dodecanoic acid 4-nitro-phenyl ester

: 250142-16-6
Hexadecanoic acid (S)-2-[12-(2,2,2-trichloro-1,1-dimethyl-ethoxycarbonylamino)-dodecanoyloxy]-3-trityloxy-propyl ester

Guidance literature:: With dmap; In chloroform; at 20 ℃; for 48h;
DOI:10.1021/jo990414e

Reference yield:

: 16975-62-5
(R)-3-(trityloxy)propane-1,2-diol

: 250142-16-6
Hexadecanoic acid (S)-2-[12-(2,2,2-trichloro-1,1-dimethyl-ethoxycarbonylamino)-dodecanoyloxy]-3-trityloxy-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 66.8 percent / DMAP / CHCl₃ / 48 h / 0 °C

2: 89.5 percent / DMAP / CHCl₃ / 48 h / 20 °C

With dmap; In chloroform; 1: Acylation / 2: Acylation;
DOI:10.1021/jo990414e

Reference yield:

: 111247-96-2
methyl (2S)-2-hydroxy-3-(triphenylmethoxy)propanoate

: 250142-16-6
Hexadecanoic acid (S)-2-[12-(2,2,2-trichloro-1,1-dimethyl-ethoxycarbonylamino)-dodecanoyloxy]-3-trityloxy-propyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 84.7 percent / LiBH₄ / tetrahydrofuran / 0 - 20 °C

2: 66.8 percent / DMAP / CHCl₃ / 48 h / 0 °C

3: 89.5 percent / DMAP / CHCl₃ / 48 h / 20 °C

With dmap; lithium borohydride; In tetrahydrofuran; chloroform; 1: Reduction / 2: Acylation / 3: Acylation;
DOI:10.1021/jo990414e