2,3-di-O-benzyl-4,6-di-tert-butylsilylene-α-D-galactopyranosyl fluoride

Base Information

Chemical Name:2,3-di-O-benzyl-4,6-di-tert-butylsilylene-α-D-galactopyranosyl fluoride
CAS No.:1163124-40-0
Molecular Formula:C₂₈H₃₉FO₅Si
Molecular Weight:502.699
Hs Code.:

Synonyms:2,3-di-O-benzyl-4,6-di-tert-butylsilylene-α-D-galactopyranosyl fluoride

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Chemical Property of 2,3-di-O-benzyl-4,6-di-tert-butylsilylene-α-D-galactopyranosyl fluoride

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Technology Process of 2,3-di-O-benzyl-4,6-di-tert-butylsilylene-α-D-galactopyranosyl fluoride

There total 1 articles about 2,3-di-O-benzyl-4,6-di-tert-butylsilylene-α-D-galactopyranosyl fluoride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 911815-94-6
phenyl 2,3-di-O-benzyl-4,6-O-di-tert-butylsilylene-1-thio-β-D-galactopyranoside

: 1163124-40-0
2,3-di-O-benzyl-4,6-di-tert-butylsilylene-α-D-galactopyranosyl fluoride

Guidance literature:: With N-Bromosuccinimide; diethylamino-sulfur trifluoride; In dichloromethane; at -15 ℃; for 1.5h;
DOI:10.1016/j.carres.2009.02.019

Reference yield: 91.0%

: 1163124-40-0
2,3-di-O-benzyl-4,6-di-tert-butylsilylene-α-D-galactopyranosyl fluoride

: 1163124-36-4
2,6-dimethylphenyl 2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl-(1->4)-3-O-benzoyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

: 1163124-41-1
2,6-dimethylphenyl 2,3-di-O-benzyl-4,6-di-tert-butylsilylene-α-D-galactopyranosyl-(1->4)-2-O-benzoyl-3,6-di-O-benzyl-β-D-galactopyranosyl-(1->4)-3-O-benzoyl-6-O-benzyl-2-deoxy-2-(2,2,2-trichloroethoxycarbonylamino)-1-thio-β-D-glucopyranoside

Guidance literature:: With Cp₂HfCl₂; silver trifluoromethanesulfonate; In dichloromethane; at -20 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.carres.2009.02.019