(2R,5S,6S)-5-amino-6-hydroxy-2-methyl-azepane-1-carboxylic acid benzyl ester hydrochloride

Base Information

Chemical Name:(2R,5S,6S)-5-amino-6-hydroxy-2-methyl-azepane-1-carboxylic acid benzyl ester hydrochloride
CAS No.:666725-97-9
Molecular Formula:C₁₅H₂₂N₂O₃*ClH
Molecular Weight:314.812
Hs Code.:

Synonyms:(2R,5S,6S)-5-amino-6-hydroxy-2-methyl-azepane-1-carboxylic acid benzyl ester hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,5S,6S)-5-amino-6-hydroxy-2-methyl-azepane-1-carboxylic acid benzyl ester hydrochloride

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Technology Process of (2R,5S,6S)-5-amino-6-hydroxy-2-methyl-azepane-1-carboxylic acid benzyl ester hydrochloride

There total 1 articles about (2R,5S,6S)-5-amino-6-hydroxy-2-methyl-azepane-1-carboxylic acid benzyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 362510-24-5
(2R,5S,6S)-5-azido-6-hydroxy-2-methyl-azepane-1-carboxylic acid benzyl ester

: 666725-97-9
(2R,5S,6S)-5-amino-6-hydroxy-2-methyl-azepane-1-carboxylic acid benzyl ester hydrochloride

Guidance literature:: (2R,5S,6S)-5-azido-6-hydroxy-2-methyl-azepane-1-carboxylic acid benzyl ester; With triphenylphosphine; In tetrahydrofuran; water; at 45 ℃;

With hydrogenchloride; In methanol; diethyl ether;

Reference yield: 66.0%

: 666725-97-9
(2R,5S,6S)-5-amino-6-hydroxy-2-methyl-azepane-1-carboxylic acid benzyl ester hydrochloride

: 115951-16-1
1-tert-butoxycarbonylaminocyclohexanecarboxylic acid

: (2R,5S,6S)-5-{[1-(1-tert-Butoxycarbonylamino-cyclohexyl)-methanoyl]-amino}-6-hydroxy-2-methyl-azepane-1-carboxylic acid benzyl ester

Guidance literature:: With 4-methyl-morpholine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; In DMF (N,N-dimethyl-formamide); at 20 ℃;