ethyl 6-O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-1-thio-β-D-galactopyranoside

Base Information

Chemical Name:ethyl 6-O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-1-thio-β-D-galactopyranoside
CAS No.:501416-35-9
Molecular Formula:C₄₈H₅₀O₁₆S
Molecular Weight:914.981
Hs Code.:

Synonyms:ethyl 6-O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-1-thio-β-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 6-O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-1-thio-β-D-galactopyranoside

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Technology Process of ethyl 6-O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-1-thio-β-D-galactopyranoside

There total 2 articles about ethyl 6-O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 139574-31-5
C₆H₁₂O₅SC₂H₄(C₇H₄O)3

: 501416-24-6
benzoxazol-2-yl 3,4,6-tri-O-acetyl-2-O-benzyl-1-thio-β-D-glucopyranoside

: 501416-35-9
ethyl 6-O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-1-thio-β-D-galactopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; at 20 ℃;
DOI:10.1016/j.tetasy.2004.11.029

Reference yield:

: 29741-69-3
3,4,6-tetra-O-acetyl-2-O-benzyl-α-D-glucopyranosyl bromide

: 501416-35-9
ethyl 6-O-(3,4,6-tri-O-acetyl-2-O-benzyl-α-D-glucopyranosyl)-2,3,4-tri-O-benzoyl-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / K₂CO₃ / acetone; toluene / 16 h / 20 °C

2: 98 percent / AgOTf / CH₂Cl₂ / 20 °C

With silver trifluoromethanesulfonate; potassium carbonate; In dichloromethane; acetone; toluene;
DOI:10.1021/ol0273452