(9Z)-11-methylretinal

Base Information

Chemical Name:(9Z)-11-methylretinal
CAS No.:135414-23-2
Molecular Formula:C₂₁H₃₀O
Molecular Weight:298.469
Hs Code.:

Synonyms:(9Z)-11-methylretinal

Suppliers and Price of (9Z)-11-methylretinal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (9Z)-11-methylretinal

Chemical Property:

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Technology Process of (9Z)-11-methylretinal

There total 1 articles about (9Z)-11-methylretinal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 3,5-dimethyl-6-oxohexa-2,4-dienenitrile

: 105480-73-7
(β-ionyl)triphenylphosphonium bromide

: C₂₁H₃₀O

: 135414-23-2
(9Z)-11-methylretinal

: 194715-64-5
all-trans-11-methylretinal

Guidance literature:: 3,5-dimethyl-6-oxohexa-2,4-dienenitrile; (β-ionyl)triphenylphosphonium bromide; With ethyloxirane; for 60h; Reflux;

With diisobutylaluminium hydride; In Petroleum ether; at -60 - 20 ℃; for 2.5h;

With water; silica gel; In Petroleum ether; at 0 ℃; for 1h;
DOI:10.1016/j.tetlet.2010.11.144