1-methyl>-2-methoxybenzene

Base Information

Chemical Name:1-methyl>-2-methoxybenzene
CAS No.:159189-64-7
Molecular Formula:C₃₀H₄₀N₂O₅
Molecular Weight:508.658
Hs Code.:

1-<bis<5-(ethooxycarbonyl)-3,4-diethyl-2-pyrrolyl>methyl>-2-methoxybenzene

Synonyms:1-methyl>-2-methoxybenzene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-methyl>-2-methoxybenzene

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Technology Process of 1-methyl>-2-methoxybenzene

There total 1 articles about 1-methyl>-2-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 97336-41-9
ethyl 3,4-diethyl-1H-pyrrole-2-carboxylate

: 135-02-4
ortho-anisaldehyde

: 159189-64-7
1-methyl>-2-methoxybenzene

Guidance literature:: With hydrogenchloride; In ethanol; Heating;
DOI:10.1246/bcsj.67.2478

Reference yield: 72.0%

: 159189-64-7
1-methyl>-2-methoxybenzene

: 159189-65-8
1--2-methoxybenzene

Guidance literature:: With sodium hydroxide; In ethylene glycol; Heating;
DOI:10.1246/bcsj.67.2478

Reference yield:

: 159189-64-7
1-methyl>-2-methoxybenzene

: 2-<15-(3,5-di-t-butylphenyl)-2,3,7,8,12,13,17,18-octaethyl-5-porphyrinyl>phenoxyacetyl-L-alanine methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 72 percent / aq. NaOH / ethane-1,2-diol / Heating

2: 1.) p-TsOH, 2.) AcONa, p-chloranil / 1.) MeOH, THF, 2.) MeOH, THF

3: 99 percent / BBr₃ / CH₂Cl₂

4: 86 percent / K₂CO₃ / acetone

5: aq. NaOH / ethanol / Heating

6: 65 percent / Et₃N, BOP / CH₂Cl₂ / 15 h / 0 °C

With sodium hydroxide; sodium acetate; boron tribromide; chloranil; potassium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; toluene-4-sulfonic acid; triethylamine; In ethanol; dichloromethane; ethylene glycol; acetone;
DOI:10.1246/bcsj.67.2478