1-p-Methoxyphenyl-7-(2,4,6-trimethylphenyl)-4-thia-7-oxo-heptan-1-ol-4,4-dioxid

Base Information

Chemical Name:1-p-Methoxyphenyl-7-(2,4,6-trimethylphenyl)-4-thia-7-oxo-heptan-1-ol-4,4-dioxid
CAS No.:99273-67-3
Molecular Formula:C₂₂H₂₈O₅S
Molecular Weight:404.527
Hs Code.:

Synonyms:1-p-Methoxyphenyl-7-(2,4,6-trimethylphenyl)-4-thia-7-oxo-heptan-1-ol-4,4-dioxid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-p-Methoxyphenyl-7-(2,4,6-trimethylphenyl)-4-thia-7-oxo-heptan-1-ol-4,4-dioxid

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Technology Process of 1-p-Methoxyphenyl-7-(2,4,6-trimethylphenyl)-4-thia-7-oxo-heptan-1-ol-4,4-dioxid

There total 1 articles about 1-p-Methoxyphenyl-7-(2,4,6-trimethylphenyl)-4-thia-7-oxo-heptan-1-ol-4,4-dioxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: β-p-Methoxybenzoyl-β'-2,4,6-trimethylbenzoyl-diethylsulfon

: 99273-67-3
1-p-Methoxyphenyl-7-(2,4,6-trimethylphenyl)-4-thia-7-oxo-heptan-1-ol-4,4-dioxid

Guidance literature:: With DMAB; In 1,4-dioxane; acetic acid; at 70 ℃; for 24h;
DOI:10.1002/ardp.19853180907

Reference yield:

: 99273-67-3
1-p-Methoxyphenyl-7-(2,4,6-trimethylphenyl)-4-thia-7-oxo-heptan-1-ol-4,4-dioxid

: β-(2,4,6-Trimethylbenzoyl)-propionitril

: 5-p-Methoxyphenyl-1,2-oxathiolan-2-oxid

Guidance literature:: With hydrogenchloride; sodium cyanide; Yield given. Multistep reaction. Yields of byproduct given; 1.) aq. EtOH, reflux, 2.) 2 d;
DOI:10.1002/ardp.19853180908