tetradodecyl-benzophenone hydrazone

Base Information

• Chemical Name: tetradodecyl-benzophenone hydrazone
• CAS No.: 910316-72-2
• Molecular Formula: C₆₁H₁₀₈N₂O₄
• Molecular Weight: 933.54

Synonyms:tetradodecyl-benzophenone hydrazone

Chemical Property of tetradodecyl-benzophenone hydrazone

Chemical Property:

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Technology Process of tetradodecyl-benzophenone hydrazone

There total 3 articles about tetradodecyl-benzophenone hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

bis-(3,4-bis-dodecyloxy-phenyl)-methanone (910316-71-1) → tetradodecyl-benzophenone hydrazone (910316-72-2)

Guidance literature:

With hydrazine hydrate; In pentan-1-ol; for 24h; Heating;

DOI:10.1021/ja0642360

Reference yield:

1,2-bisdodecyloxybenzene (42244-53-1) → tetradodecyl-benzophenone hydrazone (910316-72-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: SOCl₂ / 2 h / Heating

1.2: 83 percent / AlCl₃ / CH₂Cl₂ / 20 °C

2.1: 88 percent / NH₂NH₂*H₂O / pentan-1-ol / 24 h / Heating

With thionyl chloride; hydrazine hydrate; In pentan-1-ol;

DOI:10.1021/ja0642360

Reference yield:

3,4-didodecyloxybenzoic acid (131525-58-1) → tetradodecyl-benzophenone hydrazone (910316-72-2)

Guidance literature:

Multi-step reaction with 2 steps

1.1: SOCl₂ / 2 h / Heating

1.2: 83 percent / AlCl₃ / CH₂Cl₂ / 20 °C

2.1: 88 percent / NH₂NH₂*H₂O / pentan-1-ol / 24 h / Heating

With thionyl chloride; hydrazine hydrate; In pentan-1-ol;

DOI:10.1021/ja0642360

upstream raw materials:

bis-(3,4-bis-dodecyloxy-phenyl)-methanone

1,2-bisdodecyloxybenzene

3,4-didodecyloxybenzoic acid

Downstream raw materials:

13-[bis-(3,4-bis-dodecyloxy-phenyl)-methylene]-13H-pentacene-6-thione

13-[bis-(3,4-bis-dodecyloxy-phenyl)-methylene]-13H-pentacen-6-one

6-[bis-(3,4-bis-dodecyloxy-phenyl)-methylene]-6,13-dihydro-pentacene

C₆₁H₁₀₆N₂O₄

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