C₆₅H₆₇N₃O₁₇

Base Information

• Chemical Name: C₆₅H₆₇N₃O₁₇
• CAS No.: 1224966-38-4
• Molecular Formula: C₆₅H₆₇N₃O₁₇
• Molecular Weight: 1162.26
• Mol file: 1224966-38-4.mol

Synonyms:C₆₅H₆₇N₃O₁₇

Chemical Property of C₆₅H₆₇N₃O₁₇

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₆₅H₆₇N₃O₁₇

There total 11 articles about C₆₅H₆₇N₃O₁₇ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

(C3H4NO)3(AcOCH2C6H4)2C6C6H4CH2OH (1224966-46-4) + 2,5,8,11,18,21,24,27-octaoxa-tricyclo[26.4.0.012,17]dotriaconta-1(28),12,14,16,29,31-hexaene-14-carboxylic acid (215322-83-1) → C65H67N3O17 (1224966-38-4)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 1h;

DOI:10.1039/b926154k

Reference yield:

tert-butyl[(4-ethynylphenyl)methoxy]dimethylsilane (1093190-17-0) → C65H67N3O17 (1224966-38-4)

Guidance literature:

Multi-step reaction with 11 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1.33 h / -78 °C

1.2: 1.17 h / -78 - 20 °C

2.1: dicyclohexyl-carbodiimide / 1,4-dioxane / 0 - 20 °C

3.1: 1,4-dioxane; ethyl acetate / 2 h / 20 °C

4.1: dmap; triethylamine / dichloromethane / 9 h / 20 °C

5.1: methanol; sodium hydroxide / 0 - 20 °C

6.1: methanol; tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

7.1: pyridine / 0.5 h / 20 °C

8.1: dicobalt octacarbonyl / 1,4-dioxane / 1.5 h / 110 °C

9.1: methanol; potassium carbonate / 0.08 h / 20 °C

10.1: pyridine / 4 h / 0 °C

11.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 1 h / 20 °C

With pyridine; methanol; dmap; n-butyllithium; dicobalt octacarbonyl; tetrabutyl ammonium fluoride; potassium carbonate; triethylamine; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; hexane; dichloromethane; ethyl acetate;

DOI:10.1039/b926154k

Reference yield:

C25H33NO5SSi → C65H67N3O17 (1224966-38-4)

Guidance literature:

Multi-step reaction with 7 steps

1: methanol; sodium hydroxide / 0 - 20 °C

2: methanol; tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 20 °C

3: pyridine / 0.5 h / 20 °C

4: dicobalt octacarbonyl / 1,4-dioxane / 1.5 h / 110 °C

5: methanol; potassium carbonate / 0.08 h / 20 °C

6: pyridine / 4 h / 0 °C

7: dmap; dicyclohexyl-carbodiimide / dichloromethane / 1 h / 20 °C

With pyridine; methanol; dmap; dicobalt octacarbonyl; tetrabutyl ammonium fluoride; potassium carbonate; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; dichloromethane;

DOI:10.1039/b926154k

upstream raw materials:

tert-butyl[(4-ethynylphenyl)methoxy]dimethylsilane

C₁₈H₂₅NO₂Si

C₁₂H₁₁NO₂

C₁₄H₁₃NO₃