Benzylester-Anhydro-Cellobiose DCBB

Base Information

Chemical Name:Benzylester-Anhydro-Cellobiose DCBB
CAS No.:1374030-56-4
Molecular Formula:C₃₅H₃₇N₃O₁₁
Molecular Weight:675.692
Hs Code.:

Synonyms:Benzylester-Anhydro-Cellobiose DCBB

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Chemical Property of Benzylester-Anhydro-Cellobiose DCBB

Chemical Property:

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Technology Process of Benzylester-Anhydro-Cellobiose DCBB

There total 6 articles about Benzylester-Anhydro-Cellobiose DCBB which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: O-(2,3-di-O-benzyl-β-D-glucopyranuronicacid)-(1→4)-3-O-acetyl-1,6-anhydro-2-azido-2-deoxy-β-D-glucopyranose

: 1374030-56-4
Benzylester-Anhydro-Cellobiose DCBB

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;

Reference yield:

: 99541-24-9
O-(2,3-di-O-benzyl-β-D-glucopyranosyl)-(1->4)-3-O-acetyl-1,6-anhydro-2-azido-2-deoxy-β-D-glucopyranose

: 1374030-56-4
Benzylester-Anhydro-Cellobiose DCBB

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hypochlorite / 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / acetonitrile / 35 °C / pH 6.5 / Aqueous phosphate buffer

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dmap / dichloromethane / 16 h / 20 °C / Inert atmosphere

With sodium hypochlorite; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dmap; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In dichloromethane; acetonitrile;

Reference yield:

: C₃₃H₃₅N₃O₉

: 1374030-56-4
Benzylester-Anhydro-Cellobiose DCBB

Guidance literature:: Multi-step reaction with 4 steps

1.1: dmap / dichloromethane / 2 h / 0 - 20 °C

2.1: trifluoroacetic acid / water; tetrahydrofuran / 4 h / 0 - 20 °C

2.2: -5 - 5 °C / pH 7

3.1: sodium hypochlorite / 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / acetonitrile / 35 °C / pH 6.5 / Aqueous phosphate buffer

4.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dmap / dichloromethane / 16 h / 20 °C / Inert atmosphere

With sodium hypochlorite; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; dmap; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; In tetrahydrofuran; dichloromethane; water; acetonitrile;