(1S,6S)-6-Methyl-cyclohex-3-enecarboxylic acid ((S)-1-phenyl-ethyl)-amide

Base Information

• Chemical Name: (1S,6S)-6-Methyl-cyclohex-3-enecarboxylic acid ((S)-1-phenyl-ethyl)-amide
• CAS No.: 92344-74-6
• Molecular Formula: C₁₆H₂₁NO
• Molecular Weight: 243.349

Synonyms:(1S,6S)-6-Methyl-cyclohex-3-enecarboxylic acid ((S)-1-phenyl-ethyl)-amide

Chemical Property of (1S,6S)-6-Methyl-cyclohex-3-enecarboxylic acid ((S)-1-phenyl-ethyl)-amide

Chemical Property:

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Technology Process of (1S,6S)-6-Methyl-cyclohex-3-enecarboxylic acid ((S)-1-phenyl-ethyl)-amide

There total 3 articles about (1S,6S)-6-Methyl-cyclohex-3-enecarboxylic acid ((S)-1-phenyl-ethyl)-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(S)-1-phenyl-ethylamine (2627-86-3) + (1S,6S)-6-Methyl-cyclohex-3-enecarbonyl chloride (92284-36-1) → (1R,6R)-6-Methyl-cyclohex-3-enecarboxylic acid ((S)-1-phenyl-ethyl)-amide (92284-47-4) + (1S,6S)-6-Methyl-cyclohex-3-enecarboxylic acid ((S)-1-phenyl-ethyl)-amide (92344-74-6)

Guidance literature:

Multistep reaction;

DOI:10.1021/jo00198a012

Reference yield:

(R)-1-phenyl-ethyl-amine (3886-69-9) + (1S,6S)-6-Methyl-cyclohex-3-enecarbonyl chloride (92284-36-1) → (1R,6R)-6-Methyl-cyclohex-3-enecarboxylic acid ((R)-1-phenyl-ethyl)-amide (92284-47-4,92344-74-6) + (1S,6S)-6-Methyl-cyclohex-3-enecarboxylic acid ((R)-1-phenyl-ethyl)-amide (92284-47-4,92344-74-6)

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃;

DOI:10.1021/jo00198a012

Reference yield:

(R)-1-phenyl-ethyl-amine (3886-69-9) + (1S,6S)-6-Methyl-cyclohex-3-enecarbonyl chloride (92284-36-1) → (1R,6R)-6-Methyl-cyclohex-3-enecarboxylic acid ((R)-1-phenyl-ethyl)-amide (92284-47-4,92344-74-6) + (1S,6S)-6-Methyl-cyclohex-3-enecarboxylic acid ((R)-1-phenyl-ethyl)-amide (92284-47-4,92344-74-6)

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃;

DOI:10.1021/jo00198a012

upstream raw materials:

(R)-1-phenyl-ethyl-amine

(1S,6S)-6-Methyl-cyclohex-3-enecarbonyl chloride

(S)-1-phenyl-ethylamine

Downstream raw materials:

(1R,6R)-6-Methyl-cyclohex-3-enecarboxylic acid (2-hydroxy-ethyl)-((R)-1-phenyl-ethyl)-amide

1R,6R-(+)-6-Methyl-3-cyclohexenyl-methanol

5t-Chlor-2t-methyl-cyclohexan-1r-carbonsaeure-tert-butylester

4c-Chlor-2t-methyl-cyclohexan-1r-carbonsaeure-tert-butylester

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