1-[(1S)-2-(4-methoxybenzyloxy)-1-methylethyl]vinyl trifluoromethanesulfonate

Base Information

Chemical Name:1-[(1S)-2-(4-methoxybenzyloxy)-1-methylethyl]vinyl trifluoromethanesulfonate
CAS No.:625124-96-1
Molecular Formula:C₁₄H₁₇F₃O₅S
Molecular Weight:354.347
Hs Code.:

Synonyms:1-[(1S)-2-(4-methoxybenzyloxy)-1-methylethyl]vinyl trifluoromethanesulfonate

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Chemical Property of 1-[(1S)-2-(4-methoxybenzyloxy)-1-methylethyl]vinyl trifluoromethanesulfonate

Chemical Property:

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Technology Process of 1-[(1S)-2-(4-methoxybenzyloxy)-1-methylethyl]vinyl trifluoromethanesulfonate

There total 2 articles about 1-[(1S)-2-(4-methoxybenzyloxy)-1-methylethyl]vinyl trifluoromethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 410077-41-7
(S)-4-(4-Methoxy-benzyloxy)-3-methyl-butan-2-one

: 4-chloro-2-aminopyridyl trifluoromethanosulfonamide

: 625124-96-1
1-[(1S)-2-(4-methoxybenzyloxy)-1-methylethyl]vinyl trifluoromethanesulfonate

Guidance literature:: (S)-4-(4-Methoxy-benzyloxy)-3-methyl-butan-2-one; With lithium hexamethyldisilazane; In tetrahydrofuran; at -78 ℃; for 0.5h;

4-chloro-2-aminopyridyl trifluoromethanosulfonamide; In tetrahydrofuran; for 0.333333h;
DOI:10.1021/ja030316h

Reference yield:

: 185203-71-8
methyl (S)-N-methyl-N-methoxy-3-(4-methoxybenzyloxy)-2-methylpropanoate

: 625124-96-1
1-[(1S)-2-(4-methoxybenzyloxy)-1-methylethyl]vinyl trifluoromethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrahydrofuran; diethyl ether / 0.17 h

2.1: LiHMDS / tetrahydrofuran / 0.5 h / -78 °C

2.2: 26.0 g / tetrahydrofuran / 0.33 h

With lithium hexamethyldisilazane; In tetrahydrofuran; diethyl ether;
DOI:10.1021/ja030316h

Reference yield:

: 625124-96-1
1-[(1S)-2-(4-methoxybenzyloxy)-1-methylethyl]vinyl trifluoromethanesulfonate

: 1-((E)-(R)-4-Bromo-2-methyl-but-3-enyloxymethyl)-4-methoxy-benzene

: (S)-1-(((3-bromo-2-methylbut-3-en-1-yl)oxy)methyl)-4-methoxybenzene

Guidance literature:: 1-[(1S)-2-(4-methoxybenzyloxy)-1-methylethyl]vinyl trifluoromethanesulfonate; With tri-n-butyl-tin hydride; lithium diisopropyl amide; In tetrahydrofuran; hexane; at -48 ℃; for 0.166667h;

With N-Bromosuccinimide; In dichloromethane; at 0 ℃; for 0.166667h; Title compound not separated from byproducts;
DOI:10.1021/ja030316h