(2R,3S,4R)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-3,4-dihydro-2H-pyrrole 1-oxide

Base Information

Chemical Name:(2R,3S,4R)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-3,4-dihydro-2H-pyrrole 1-oxide
CAS No.:1105054-49-6
Molecular Formula:C₂₆H₂₇NO₄
Molecular Weight:417.505
Hs Code.:

Synonyms:(2R,3S,4R)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-3,4-dihydro-2H-pyrrole 1-oxide

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Chemical Property of (2R,3S,4R)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-3,4-dihydro-2H-pyrrole 1-oxide

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Technology Process of (2R,3S,4R)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-3,4-dihydro-2H-pyrrole 1-oxide

There total 6 articles about (2R,3S,4R)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-3,4-dihydro-2H-pyrrole 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 16838-89-4,17073-88-0,60933-68-8,60933-69-9,73068-66-3,89361-52-4,89615-42-9,89615-45-2,96192-07-3
2,3,5-tri-O-benzyl-α-L-ribofuranose

: 1105054-49-6
(2R,3S,4R)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-3,4-dihydro-2H-pyrrole 1-oxide

Guidance literature:: 2,3,5-tri-O-benzyl-α-L-ribofuranose; With hydroxylamine hydrochloride; sodium methylate; In methanol; at 20 ℃; for 5h;

With 1H-imidazole; tert-butylchlorodiphenylsilane; In dichloromethane; at 20 ℃; for 2h; Further stages;
DOI:10.1016/j.ejmech.2016.07.025

Reference yield: 45.0%

: C₂₆H₂₈O₅

: 1105054-49-6
(2R,3S,4R)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-3,4-dihydro-2H-pyrrole 1-oxide

Guidance literature:: C₂₆H₂₈O₅; With hydroxylamine hydrochloride; sodium methylate; In methanol; at 20 ℃; for 5h;

With 1H-imidazole; tert-butylchlorodiphenylsilane; In dichloromethane; at 20 ℃; for 2h; Further stages;

Reference yield:

: C₂₆H₂₉NO₅

: 1105054-49-6
(2R,3S,4R)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-3,4-dihydro-2H-pyrrole 1-oxide

Guidance literature:: C₂₆H₂₉NO₅; With 1H-imidazole; tert-butylchlorodiphenylsilane; In dichloromethane; at 20 ℃; for 2h;

With methanesulfonyl chloride; triethylamine; In dichloromethane; at 0 ℃; for 3h; Further stages;
DOI:10.1016/j.ejmech.2016.10.004