N4,N6-dimethyl-N2-methyl-N2-(3',5'-di-O-triisopropylsilyl-2'-deoxy-β-D-erythro-pentofuranosyl)-[1,3,5]triazine-2,4,6-triamine

Base Information

Chemical Name:N4,N6-dimethyl-N2-methyl-N2-(3',5'-di-O-triisopropylsilyl-2'-deoxy-β-D-erythro-pentofuranosyl)-[1,3,5]triazine-2,4,6-triamine
CAS No.:865452-48-8
Molecular Formula:C₂₉H₆₀N₆O₃Si₂
Molecular Weight:597.005
Hs Code.:

Synonyms:N4,N6-dimethyl-N2-methyl-N2-(3',5'-di-O-triisopropylsilyl-2'-deoxy-β-D-erythro-pentofuranosyl)-[1,3,5]triazine-2,4,6-triamine

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Chemical Property of N4,N6-dimethyl-N2-methyl-N2-(3',5'-di-O-triisopropylsilyl-2'-deoxy-β-D-erythro-pentofuranosyl)-[1,3,5]triazine-2,4,6-triamine

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Technology Process of N4,N6-dimethyl-N2-methyl-N2-(3',5'-di-O-triisopropylsilyl-2'-deoxy-β-D-erythro-pentofuranosyl)-[1,3,5]triazine-2,4,6-triamine

There total 1 articles about N4,N6-dimethyl-N2-methyl-N2-(3',5'-di-O-triisopropylsilyl-2'-deoxy-β-D-erythro-pentofuranosyl)-[1,3,5]triazine-2,4,6-triamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 865452-45-5
N4,N6-dimethyl-N2-methyl-N2-(5'-O-triisopropylsilyl-2'-deoxy-β-D-erythro-pentofuranosyl)-[1,3,5]triazine-2,4,6-triamine

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 865452-48-8
N4,N6-dimethyl-N2-methyl-N2-(3',5'-di-O-triisopropylsilyl-2'-deoxy-β-D-erythro-pentofuranosyl)-[1,3,5]triazine-2,4,6-triamine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 0.25h; cooling;
DOI:10.1039/b503757c

Reference yield:

: 865452-48-8
N4,N6-dimethyl-N2-methyl-N2-(3',5'-di-O-triisopropylsilyl-2'-deoxy-β-D-erythro-pentofuranosyl)-[1,3,5]triazine-2,4,6-triamine

: N4,N6-diisobutyryl-N4,N6-dimethyl-N2-methyl-N2-(5'-O-(4,4'-dimethoxytriphenylmethyl)-2'-deoxy-β-D-erythro-pentofuranosyl)-[1,3,5]triazine-2,4,6-triamine

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / DMAP / 1,2-dichloro-ethane / 3 h / 60 °C

2: 88 percent / TBAF / tetrahydrofuran / 0.25 h / 20 °C

3: 91 percent / DIPEA / CH₂Cl₂ / 2 h / 20 °C

With dmap; tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; 1,2-dichloro-ethane;
DOI:10.1039/b503757c