Technology Process of C37H48N5O14PS
There total 14 articles about C37H48N5O14PS which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
dmap; dicyclohexyl-carbodiimide;
In
dichloromethane; N,N-dimethyl-formamide;
at 0 - 20 ℃;
for 24h;
Inert atmosphere;
DOI:10.1002/ejoc.201301781
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sodium hydrogencarbonate / tetrahydrofuran; water / 16 h / 0 - 20 °C / Inert atmosphere
2: palladium 10% on activated carbon; hydrogen / ethanol / 16 h / 0 - 20 °C / 760.05 Torr
3: dmap; dicyclohexyl-carbodiimide / dichloromethane; N,N-dimethyl-formamide / 24 h / 0 - 20 °C / Inert atmosphere
With
dmap; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; dicyclohexyl-carbodiimide;
In
tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201301781
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 1H-tetrazole / dichloromethane; acetonitrile / 12 h / 0 - 20 °C / Inert atmosphere
1.2: 2 h / -40 - 20 °C / Inert atmosphere
2.1: methylamine / water; ethanol / 0.5 h / 0 - 20 °C
3.1: dmap; dicyclohexyl-carbodiimide / dichloromethane; N,N-dimethyl-formamide / 24 h / 0 - 20 °C / Inert atmosphere
With
1H-tetrazole; dmap; dicyclohexyl-carbodiimide; methylamine;
In
ethanol; dichloromethane; water; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/ejoc.201301781
