(+)-(1'R,2R,3R,S_S)-3-n-butyl-2-(1'-hydroxypropyl)-2-(p-tolylsulfinyl)oxirane

Base Information

• Chemical Name: (+)-(1'R,2R,3R,S_S)-3-n-butyl-2-(1'-hydroxypropyl)-2-(p-tolylsulfinyl)oxirane
• CAS No.: 182879-13-6
• Molecular Formula: C₁₆H₂₄O₃S
• Molecular Weight: 296.431

Synonyms:(+)-(1'R,2R,3R,S_S)-3-n-butyl-2-(1'-hydroxypropyl)-2-(p-tolylsulfinyl)oxirane

Chemical Property of (+)-(1'R,2R,3R,S_S)-3-n-butyl-2-(1'-hydroxypropyl)-2-(p-tolylsulfinyl)oxirane

Chemical Property:

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Technology Process of (+)-(1'R,2R,3R,S_S)-3-n-butyl-2-(1'-hydroxypropyl)-2-(p-tolylsulfinyl)oxirane

There total 2 articles about (+)-(1'R,2R,3R,S_S)-3-n-butyl-2-(1'-hydroxypropyl)-2-(p-tolylsulfinyl)oxirane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 6.0%

(E)-4(SS)-(p-tolylsulfinyl)pent-4-en-3(R)-ol (131973-93-8,131973-90-5) → (+)-(1'R,2R,3R,SS)-3-n-butyl-2-(1'-hydroxypropyl)-2-(p-tolylsulfinyl)oxirane (182879-13-6) + (-)-(1'R,2R,3R)-3-n-butyl-2-(1'-hydroxypropyl)-2-(p-tolylsulfonyl)oxirane + (-)-(2S,3S)-3-(n-butyl)-2-((1R)-1-hydroxypropyl)-2-(p-tolylsulfonyl)oxirane

Guidance literature:

With tert.-butylhydroperoxide; sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.75h; Further Variations:; Reagents; Solvents; Product distribution;

DOI:10.1021/jo026182s

Reference yield:

(E)-4(SS)-(p-tolylsulfinyl)pent-4-en-3(R)-ol (131973-93-8,131973-90-5) → (+)-(1'R,2R,3R,SS)-3-n-butyl-2-(1'-hydroxypropyl)-2-(p-tolylsulfinyl)oxirane (182879-13-6) + (R)-1-[3-Butyl-2-(toluene-4-sulfonyl)-oxiranyl]-propan-1-ol

Guidance literature:

With KOO-t-Bu; In tetrahydrofuran; at 0 ℃; for 0.416667h; Yield given. Yields of byproduct given;

DOI:10.1016/S0040-4039(96)01481-5

Reference yield: 67.0%

(+)-(1'R,2R,3R,SS)-3-n-butyl-2-(1'-hydroxypropyl)-2-(p-tolylsulfinyl)oxirane (182879-13-6) → (+)-(1'R,2R,3R,SS)-3-n-butyl-2-(1'-hydroxypropyl)-2-(p-tolylsulfinyl)oxirane p-nitrobenzoate

Guidance literature:

(+)-(1'R,2R,3R,S_S)-3-n-butyl-2-(1'-hydroxypropyl)-2-(p-tolylsulfinyl)oxirane; With dmap; triethylamine; In tetrahydrofuran; at 0 ℃; for 0.166667h; Further stages.;

DOI:10.1021/jo026182s

upstream raw materials:

(E)-4(S_S)-(p-tolylsulfinyl)pent-4-en-3(R)-ol

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