4-Bromo-2,6-diethylbenzoic acid

Base Information

Chemical Name:4-Bromo-2,6-diethylbenzoic acid
CAS No.:1349716-04-6
Molecular Formula:C₁₁H₁₃BrO₂
Molecular Weight:257.127
Hs Code.:
DSSTox Substance ID:DTXSID001304649

Synonyms:4-Bromo-2,6-diethylbenzoic acid;1349716-04-6;4-Bromo-2,6-diethylbenzoicacid;SCHEMBL15328457;XPAXESMAIOZLJT-UHFFFAOYSA-N;DTXSID001304649;4-bromo-2,6-diethyl-benzoic acid

Suppliers and Price of 4-Bromo-2,6-diethylbenzoic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 1 raw suppliers

Chemical Property of 4-Bromo-2,6-diethylbenzoic acid

Chemical Property:

XLogP3:3.7
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:256.00989
Heavy Atom Count:14
Complexity:192

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CCC1=CC(=CC(=C1C(=O)O)CC)Br

Technology Process of 4-Bromo-2,6-diethylbenzoic acid

There total 3 articles about 4-Bromo-2,6-diethylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1472104-61-2
4-bromo-2,6-diethyl-N-quinolin-8-yl-benzamide

: 1349716-04-6
4-bromo-2,6-diethyl-benzoic acid

Guidance literature:: With sulfuric acid; at 120 ℃; for 16h;

Reference yield:

: 586-75-4
4-chlorobenzoyl chloride

: 1349716-04-6
4-bromo-2,6-diethyl-benzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / dichloromethane / 16 h / 23 °C

2: palladium diacetate; Trimethylacetic acid; potassium carbonate / tert-Amyl alcohol / 48.5 h / 100 °C / Sealed tube; Inert atmosphere

3: sulfuric acid / 16 h / 120 °C

With sulfuric acid; palladium diacetate; potassium carbonate; triethylamine; Trimethylacetic acid; In tert-Amyl alcohol; dichloromethane;

Reference yield:

: 299928-52-2
4-bromo-N-quinolin-8-ylbenzamide

: 1349716-04-6
4-bromo-2,6-diethyl-benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: palladium diacetate; Trimethylacetic acid; potassium carbonate / tert-Amyl alcohol / 48.5 h / 100 °C / Sealed tube; Inert atmosphere

2: sulfuric acid / 16 h / 120 °C

With sulfuric acid; palladium diacetate; potassium carbonate; Trimethylacetic acid; In tert-Amyl alcohol;