Technology Process of C23H32N2O4Si
There total 8 articles about C23H32N2O4Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; triphenyl-arsane;
In
N,N-dimethyl-formamide;
at 20 ℃;
DOI:10.1039/c3sc00056g
- Guidance literature:
-
Multi-step reaction with 2 steps
1: toluene / 100 °C
2: tris(dibenzylideneacetone)dipalladium(0) chloroform complex; triphenyl-arsane / N,N-dimethyl-formamide / 20 °C
With
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; triphenyl-arsane;
In
N,N-dimethyl-formamide; toluene;
2: |Stille Cross Coupling;
DOI:10.1039/c3sc00056g
- Guidance literature:
-
Multi-step reaction with 7 steps
1: diethyl ether / -10 °C
2: pyridine; dmap / dichloromethane / 0 °C
3: lithium diisopropyl amide; N,N,N,N,N,N-hexamethylphosphoric triamide / tetrahydrofuran / -78 °C
4: acetyl chloride / 20 °C
5: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / -10 °C
6: toluene / 100 °C
7: tris(dibenzylideneacetone)dipalladium(0) chloroform complex; triphenyl-arsane / N,N-dimethyl-formamide / 20 °C
With
pyridine; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; tris(dibenzylideneacetone)dipalladium(0) chloroform complex; triphenyl-arsane; di-isopropyl azodicarboxylate; acetyl chloride; triphenylphosphine; lithium diisopropyl amide;
In
tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide; toluene;
3: |Claisen-Ireland Rearrangement / 5: |Mitsunobu Displacement / 7: |Stille Cross Coupling;
DOI:10.1039/c3sc00056g
