2-chloro-5-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-1,3,4-thiadiazole

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Chemical Name:2-chloro-5-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-1,3,4-thiadiazole
CAS No.:1225430-45-4
Molecular Formula:C₄₃H₄₀Cl₂N₂O₅S
Molecular Weight:767.773
Hs Code.:

Synonyms:2-chloro-5-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-1,3,4-thiadiazole

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Chemical Property of 2-chloro-5-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-1,3,4-thiadiazole

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Technology Process of 2-chloro-5-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-1,3,4-thiadiazole

There total 2 articles about 2-chloro-5-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-1,3,4-thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 1225430-97-6
5-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-1,3,4-thiadiazol-2-amine

: 1225430-45-4
2-chloro-5-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-1,3,4-thiadiazole

Guidance literature:: With hydrogenchloride; sodium nitrite; copper; In water; acetic acid; at 0 - 20 ℃; for 3h;

Reference yield: 22.0%

: 1225430-40-9
2-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)phenyl)acetic acid

: 79-19-6
thiosemicarbazide

: 1225430-45-4
2-chloro-5-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-1,3,4-thiadiazole

Guidance literature:: 2-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)phenyl)acetic acid; thiosemicarbazide; In 1,4-dioxane; at 90 ℃; for 1h; Inert atmosphere;

With trichlorophosphate; In 1,4-dioxane; at 110 ℃; Inert atmosphere;

With hydrogenchloride; copper; acetic acid; sodium nitrite; In water; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2010.01.073

Reference yield: 77.0%

: 1225430-45-4
2-chloro-5-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-1,3,4-thiadiazole

: 5188-07-8
sodium thiomethoxide

: 1225430-98-7
2-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-5-methylthio-1,3,4-thiadiazole

Guidance literature:: 2-chloro-5-(2-chloro-5-((2S,3S,4R,5R,6R)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)tetrahydro-2H-pyran-2-yl)benzyl)-1,3,4-thiadiazole; sodium thiomethoxide; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

With hydrogenchloride; In tetrahydrofuran; water; at 0 ℃;