5-benzyl-1,3-dimethylurea-4-hydrotriazinium bromide

Base Information

Chemical Name:5-benzyl-1,3-dimethylurea-4-hydrotriazinium bromide
CAS No.:1360616-69-8
Molecular Formula:Br*C₁₂H₁₆N₃O
Molecular Weight:298.183
Hs Code.:

Synonyms:5-benzyl-1,3-dimethylurea-4-hydrotriazinium bromide

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Chemical Property of 5-benzyl-1,3-dimethylurea-4-hydrotriazinium bromide

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Technology Process of 5-benzyl-1,3-dimethylurea-4-hydrotriazinium bromide

There total 1 articles about 5-benzyl-1,3-dimethylurea-4-hydrotriazinium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 911857-60-8
5-benzyl-1,3-dimethyl-[1,3,5]triazinan-2-one

: 1360616-69-8
5-benzyl-1,3-dimethylurea-4-hydrotriazinium bromide

Guidance literature:: With N-Bromosuccinimide; In 1,2-dimethoxyethane; at 20 ℃; for 0.75h;
DOI:10.1021/om201275z

Reference yield: 71.0%

: chloro(1,5-cyclooctadiene)rhodium(I) dimer

: 1360616-69-8
5-benzyl-1,3-dimethylurea-4-hydrotriazinium bromide

: bromo-1,5-cyclooctadiene-5-benzyl-1,3-dimethylurea-4-hydrotriazin-2-ylidenerhodium(I)

Guidance literature:: With KOC(CH₃)3; In tetrahydrofuran; (under N2, Schlenk); ligand, KOC(CH3)3 and Rh-complex placed in flask, cooled to -80°C, 10 min, THF added dropwise with stirring, stirredfor 30 min at -80°C, warmed to room temp., stirred overnight; solvent removed in vacuo, flask chromy. on silica with THF, volatiles evapd. in vacuo; elem. anal.;
DOI:10.1021/om201275z

Reference yield: 71.0%

: 12112-67-3
bis(1,5-cyclooctadiene)diiridium(I) dichloride

: 1360616-69-8
5-benzyl-1,3-dimethylurea-4-hydrotriazinium bromide

: bromo-1,5-cyclooctadiene-5-benzyl-1,3-dimethylurea-4-hydrotriazin-2-ylideneiridium(I)

Guidance literature:: With KOC(CH₃)3; In tetrahydrofuran; (under N2, Schlenk); ligand, KOC(CH3)3 and Ir-complex placed in flask, cooled to -80°C, 10 min, THF added dropwise with stirring, stirredfor 30 min at -80°C, warmed to room temp., stirred overnight; solvent removed in vacuo, flask chromy. on silica with THF, volatiles evapd. in vacuo; elem. anal.;
DOI:10.1021/om201275z