(1S)-1,5-anhydro-2,3,4,6-tetra-O-benzyl-1-[2-(benzyloxy)-5-(4-chloro-2-methylbenzyl)-4-methylphenyl]-1-thio-D-glucitol

Base Information

• Chemical Name: (1S)-1,5-anhydro-2,3,4,6-tetra-O-benzyl-1-[2-(benzyloxy)-5-(4-chloro-2-methylbenzyl)-4-methylphenyl]-1-thio-D-glucitol
• CAS No.: 1000369-10-7
• Molecular Formula: C₅₆H₅₅ClO₅S
• Molecular Weight: 875.569

Synonyms:(1S)-1,5-anhydro-2,3,4,6-tetra-O-benzyl-1-[2-(benzyloxy)-5-(4-chloro-2-methylbenzyl)-4-methylphenyl]-1-thio-D-glucitol

Chemical Property of (1S)-1,5-anhydro-2,3,4,6-tetra-O-benzyl-1-[2-(benzyloxy)-5-(4-chloro-2-methylbenzyl)-4-methylphenyl]-1-thio-D-glucitol

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Technology Process of (1S)-1,5-anhydro-2,3,4,6-tetra-O-benzyl-1-[2-(benzyloxy)-5-(4-chloro-2-methylbenzyl)-4-methylphenyl]-1-thio-D-glucitol

There total 1 articles about (1S)-1,5-anhydro-2,3,4,6-tetra-O-benzyl-1-[2-(benzyloxy)-5-(4-chloro-2-methylbenzyl)-4-methylphenyl]-1-thio-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C56H55ClO7S (1000369-11-8) → (1S)-1,5-anhydro-2,3,4,6-tetra-O-benzyl-1-[2-(benzyloxy)-5-(4-chloro-2-methylbenzyl)-4-methylphenyl]-1-thio-D-glucitol (1000369-10-7)

Guidance literature:

With triethylsilane; boron trifluoride diethyl etherate; In chloroform; acetonitrile; at 0 - 20 ℃; for 2h;

Reference yield:

but-3-enoic acid (625-38-7) + (1S)-1,5-anhydro-2,3,4,6-tetra-O-benzyl-1-[2-(benzyloxy)-5-(4-chloro-2-methylbenzyl)-4-methylphenyl]-1-thio-D-glucitol (1000369-10-7) → C60H60O7S (1000369-18-5)

Guidance literature:

With caesium carbonate; (bis(tricyclohexyl)phosphine)palladium(II) dichloride; In 1,4-dioxane; at 160 ℃; for 2h; Microwave irradiation;

upstream raw materials:

C₅₆H₅₅ClO₇S

Downstream raw materials:

C₆₀H₆₀O₇S

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