dodecahydro-1,4:5,8-dimethanoanthracene-9,10-dione

Base Information

• Chemical Name: dodecahydro-1,4:5,8-dimethanoanthracene-9,10-dione
• CAS No.: 66513-31-3
• Molecular Formula: C₁₆H₂₀O₂
• Molecular Weight: 244.334

Synonyms:NSC 245079

Chemical Property of dodecahydro-1,4:5,8-dimethanoanthracene-9,10-dione

Chemical Property:

• Vapor Pressure: 1.09E-06mmHg at 25°C
• Boiling Point: 402.5°Cat760mmHg
• Flash Point: 150.8°C
• Density: 1.216g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

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Technology Process of dodecahydro-1,4:5,8-dimethanoanthracene-9,10-dione

There total 13 articles about dodecahydro-1,4:5,8-dimethanoanthracene-9,10-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 15.0%

endo-cis-anti-cis-endo-1,2,3,4,4a,5,6,7,8,8a,9a,10a-Dodecahydro-1,4:5,8-dimethanoanthracene-9,10-dione (2065-48-7) → endo-cis-syn-cis-exo-1,2,3,4,4a,5,6,7,8,8a,9a,10a-Dodecahydro-1,4:5,8-dimethanoanthracene-9,10-dione (2065-48-7,66513-31-3,130855-39-9,130855-45-7,130855-47-9)

Guidance literature:

at 240 ℃; for 0.0833333h;

Reference yield:

Cyclopentadiene-p-benzoquinone Diels-Alder adduct (5439-22-5) → Dodecahydro-1,4:5,8-dimethano-9,10-anthraquinone (66513-31-3,130855-39-9,130855-45-7,130855-47-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; ethyl acetate; for 3h; under 2585.7 Torr; Yield given;

DOI:10.1021/jo00119a017

Reference yield:

1α,4α,4aα,10aα,5β,8β,8aα,9aα-octahydro-1,4:5,8-dimethanoanthracene-9,10-dione (130855-42-4) → endo-cis-syn-cis-exo-1,2,3,4,4a,5,6,7,8,8a,9a,10a-Dodecahydro-1,4:5,8-dimethanoanthracene-9,10-dione (2065-48-7,66513-31-3,130855-39-9,130855-45-7,130855-47-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; for 2h; under 760 Torr; Ambient temperature;

upstream raw materials:

Cyclopentadiene-p-benzoquinone Diels-Alder adduct

endo-cis-anti-cis-endo-1,2,3,4,4a,5,6,7,8,8a,9a,10a-Dodecahydro-1,4:5,8-dimethanoanthracene-9,10-dione

1α,4α,4aα,10aα,5β,8β,8aα,9aα-octahydro-1,4:5,8-dimethanoanthracene-9,10-dione

1α,4α,4aβ,10aα,5β,8β,8aα,9aβ-octahydro-1,4:5,8-dimethanoanthracene-9,10-dione

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