6-(4-chloro-benzenesulfonyl)-8-cyclopentyl-2-methylsulfinyl-8Hpyrido[2,3-d]pyrimidin-7-one

Base Information

Chemical Name:6-(4-chloro-benzenesulfonyl)-8-cyclopentyl-2-methylsulfinyl-8Hpyrido[2,3-d]pyrimidin-7-one
CAS No.:1312471-69-4
Molecular Formula:C₁₉H₁₈ClN₃O₄S₂
Molecular Weight:451.955
Hs Code.:

Synonyms:6-(4-chloro-benzenesulfonyl)-8-cyclopentyl-2-methylsulfinyl-8Hpyrido[2,3-d]pyrimidin-7-one

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Chemical Property of 6-(4-chloro-benzenesulfonyl)-8-cyclopentyl-2-methylsulfinyl-8Hpyrido[2,3-d]pyrimidin-7-one

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Technology Process of 6-(4-chloro-benzenesulfonyl)-8-cyclopentyl-2-methylsulfinyl-8Hpyrido[2,3-d]pyrimidin-7-one

There total 10 articles about 6-(4-chloro-benzenesulfonyl)-8-cyclopentyl-2-methylsulfinyl-8Hpyrido[2,3-d]pyrimidin-7-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1312471-70-7
6-(4-chlorobenzenesulfonyl)-8-cyclopentyl-2-methylsulfanyl-8H-pyrido[2,3-d]pyrimidin-7-one

: 1312471-69-4
6-(4-chloro-benzenesulfonyl)-8-cyclopentyl-2-methylsulfinyl-8Hpyrido[2,3-d]pyrimidin-7-one

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 4h;
DOI:10.1021/jm401073p

Reference yield:

: 3405-89-8
2-(4-chloro-phenylsulfonyl)acetic acid

: 1312471-69-4
6-(4-chloro-benzenesulfonyl)-8-cyclopentyl-2-methylsulfinyl-8Hpyrido[2,3-d]pyrimidin-7-one

Guidance literature:: Multi-step reaction with 2 steps

1: benzylamine; acetic acid / 6 h / 100 °C

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 20 °C

With acetic acid; 3-chloro-benzenecarboperoxoic acid; benzylamine; In dichloromethane;
DOI:10.1021/jm401073p

Reference yield:

: 1003-03-8
Cyclopentamine

: 1312471-69-4
6-(4-chloro-benzenesulfonyl)-8-cyclopentyl-2-methylsulfinyl-8Hpyrido[2,3-d]pyrimidin-7-one

Guidance literature:: Multi-step reaction with 5 steps

1: triethylamine / tetrahydrofuran / 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / -10 - 20 °C / Inert atmosphere

3: manganese(IV) oxide / chloroform / 24 h / 20 °C

4: benzylamine; acetic acid / 6 h / 100 °C

5: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 4 h / 20 °C

With manganese(IV) oxide; lithium aluminium tetrahydride; acetic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; benzylamine; In tetrahydrofuran; dichloromethane; chloroform;
DOI:10.1021/jm401073p