acetic acid 1-(4,5-dimethoxy-2-nitrobenzyloxy)-3-methylsulfanylpropyl ester

Base Information

Chemical Name:acetic acid 1-(4,5-dimethoxy-2-nitrobenzyloxy)-3-methylsulfanylpropyl ester
CAS No.:863608-03-1
Molecular Formula:C₁₅H₂₁NO₇S
Molecular Weight:359.4
Hs Code.:

Synonyms:acetic acid 1-(4,5-dimethoxy-2-nitrobenzyloxy)-3-methylsulfanylpropyl ester

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Chemical Property of acetic acid 1-(4,5-dimethoxy-2-nitrobenzyloxy)-3-methylsulfanylpropyl ester

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Technology Process of acetic acid 1-(4,5-dimethoxy-2-nitrobenzyloxy)-3-methylsulfanylpropyl ester

There total 2 articles about acetic acid 1-(4,5-dimethoxy-2-nitrobenzyloxy)-3-methylsulfanylpropyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 3-methylsulfanylpropionic acid 4,5-dimethoxy-2-nitrobenzyl ester

: 108-24-7
acetic anhydride

: 863608-03-1
acetic acid 1-(4,5-dimethoxy-2-nitrobenzyloxy)-3-methylsulfanylpropyl ester

Guidance literature:: 3-methylsulfanylpropionic acid 4,5-dimethoxy-2-nitrobenzyl ester; With diisobutylaluminium hydride; In hexane; dichloromethane; at -78 ℃; for 0.75h;

acetic anhydride; With pyridine; dmap; In hexane; dichloromethane; at -78 - 0 ℃;
DOI:10.1021/ol051280w

Reference yield:

: 1016-58-6
6-nitroveratryl alcohol

: 863608-03-1
acetic acid 1-(4,5-dimethoxy-2-nitrobenzyloxy)-3-methylsulfanylpropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 89 percent / Et₃N; 4-dimethylaminopyridine / CH₂Cl₂ / 20 h / 25 °C

2.1: DIBAL-H / CH₂Cl₂; hexane / 0.75 h / -78 °C

2.2: 77 percent / 4-dimethylaminopyridine; pyridine / CH₂Cl₂; hexane / -78 - 0 °C

With dmap; diisobutylaluminium hydride; triethylamine; In hexane; dichloromethane;
DOI:10.1021/ol051280w