methoxycarbonylmethyl 2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

Base Information

Chemical Name:methoxycarbonylmethyl 2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside
CAS No.:503173-61-3
Molecular Formula:C₅₇H₆₂O₁₂S
Molecular Weight:971.178
Hs Code.:

Synonyms:methoxycarbonylmethyl 2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

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Chemical Property of methoxycarbonylmethyl 2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

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Technology Process of methoxycarbonylmethyl 2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

There total 6 articles about methoxycarbonylmethyl 2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 441017-72-7
methoxycarbonylmethyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

: 503173-61-3
methoxycarbonylmethyl 2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

Guidance literature:: With sodium methylate; In methanol; at 20 ℃;

Reference yield:

: 3879-79-6,17791-37-6,19488-61-0,53008-63-2,61330-62-9,69237-94-1,69237-95-2,71526-33-5,83462-67-3,84799-77-9,103421-29-0,103421-30-3,139241-42-2
methyl 2,3,4,6-tetra-O-benzyl-α-D-glucopyranoside

: 503173-61-3
methoxycarbonylmethyl 2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1: ZnCl₂ / acetic acid / 4 h / 20 °C

2: 100 percent / iodo trimethylsilane / CH₂Cl₂ / 2 h / 0 °C

3: 88 percent / tetrabutylammonium idide; diisopropylethylamine / benzene / 4 h / Heating

4: 98 percent / NaOMe / methanol / 20 °C

With trimethylsilyl iodide; sodium methylate; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; zinc(II) chloride; In methanol; dichloromethane; acetic acid; benzene;

Reference yield:

: 4356-77-8
acetyl 6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranoside

: 503173-61-3
methoxycarbonylmethyl 2,3,4-tri-O-benzyl-α-D-glucopyranosyl-(1->6)-2,3,4-tri-O-benzyl-1-thio-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / iodo trimethylsilane / CH₂Cl₂ / 2 h / 0 °C

2: 88 percent / tetrabutylammonium idide; diisopropylethylamine / benzene / 4 h / Heating

3: 98 percent / NaOMe / methanol / 20 °C

With trimethylsilyl iodide; sodium methylate; tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; benzene;