2,6-dichloro-1-(2-methoxy-ethoxymethyl)-5-m-tolylsulfanyl-1H-benzoimidazole

Base Information

Chemical Name:2,6-dichloro-1-(2-methoxy-ethoxymethyl)-5-m-tolylsulfanyl-1H-benzoimidazole
CAS No.:1193384-37-0
Molecular Formula:C₁₈H₁₈Cl₂N₂O₂S
Molecular Weight:397.325
Hs Code.:

Synonyms:2,6-dichloro-1-(2-methoxy-ethoxymethyl)-5-m-tolylsulfanyl-1H-benzoimidazole

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Chemical Property of 2,6-dichloro-1-(2-methoxy-ethoxymethyl)-5-m-tolylsulfanyl-1H-benzoimidazole

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Technology Process of 2,6-dichloro-1-(2-methoxy-ethoxymethyl)-5-m-tolylsulfanyl-1H-benzoimidazole

There total 5 articles about 2,6-dichloro-1-(2-methoxy-ethoxymethyl)-5-m-tolylsulfanyl-1H-benzoimidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3970-21-6
2-Methoxyethoxymethyl chloride

: 1193384-35-8
6-chloro-5-m-tolylsulfanyl-1H-benzoimidazole

: 1193384-37-0
2,6-dichloro-1-(2-methoxy-ethoxymethyl)-5-m-tolylsulfanyl-1H-benzoimidazole

: 1193385-58-8
C₁₈H₁₈Cl₂N₂O₂S

Guidance literature:: 2-Methoxyethoxymethyl chloride; 6-chloro-5-m-tolylsulfanyl-1H-benzoimidazole; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 0 - 23 ℃;

With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; Cooling with acetone-dry ice;

With N-chloro-succinimide; In tetrahydrofuran; at 23 ℃;

Reference yield:

: 1193384-34-7
4-chloro-5-m-tolylsulfanyl-benzene-1,2-diamine

: 1193384-37-0
2,6-dichloro-1-(2-methoxy-ethoxymethyl)-5-m-tolylsulfanyl-1H-benzoimidazole

: 1193385-58-8
C₁₈H₁₈Cl₂N₂O₂S

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / 16 h / 23 °C

2.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 23 °C

2.2: -78 °C / Cooling with acetone-dry ice

2.3: 23 °C

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;

Reference yield:

: 108-40-7
toluene-3-thiol

: 1193384-37-0
2,6-dichloro-1-(2-methoxy-ethoxymethyl)-5-m-tolylsulfanyl-1H-benzoimidazole

: 1193385-58-8
C₁₈H₁₈Cl₂N₂O₂S

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 16 h / 90 °C

2.1: ammonium chloride; zinc / water; acetone / 0 °C

3.1: hydrogenchloride / 16 h / 23 °C

4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 0 - 23 °C

4.2: -78 °C / Cooling with acetone-dry ice

4.3: 23 °C

With hydrogenchloride; potassium carbonate; ammonium chloride; N-ethyl-N,N-diisopropylamine; zinc; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetone;