(1S,2S,3R,4R,5S,6S)-2,3,4,5-tetrakis(benzyloxy)-6-(nonylamino)cyclohexanol

Base Information

Chemical Name:(1S,2S,3R,4R,5S,6S)-2,3,4,5-tetrakis(benzyloxy)-6-(nonylamino)cyclohexanol
CAS No.:1287225-51-7
Molecular Formula:C₄₃H₅₅NO₅
Molecular Weight:665.913
Hs Code.:

Synonyms:(1S,2S,3R,4R,5S,6S)-2,3,4,5-tetrakis(benzyloxy)-6-(nonylamino)cyclohexanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (1S,2S,3R,4R,5S,6S)-2,3,4,5-tetrakis(benzyloxy)-6-(nonylamino)cyclohexanol

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Technology Process of (1S,2S,3R,4R,5S,6S)-2,3,4,5-tetrakis(benzyloxy)-6-(nonylamino)cyclohexanol

There total 1 articles about (1S,2S,3R,4R,5S,6S)-2,3,4,5-tetrakis(benzyloxy)-6-(nonylamino)cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 124-19-6
nonan-1-al

: 1198207-03-2
(1S,2S,3S,4R,5R,6S)-2-amino-3,4,5,6-tetrakis(benzyloxy)cyclohexanol

: 1287225-51-7
(1S,2S,3R,4R,5S,6S)-2,3,4,5-tetrakis(benzyloxy)-6-(nonylamino)cyclohexanol

Guidance literature:: With sodium cyanoborohydride; acetic acid; In methanol; at 20 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ja111480z

Reference yield: 74.0%

: 4430-43-7
n-nonyl isothiocyanate

: 1287225-51-7
(1S,2S,3R,4R,5S,6S)-2,3,4,5-tetrakis(benzyloxy)-6-(nonylamino)cyclohexanol

: 1287225-70-0
1,3-dinonyl-1-((1S,2S,3R,4R,5S,6S)-2,3,4,5-tetrakis(benzyloxy)-6-hydroxycyclohexyl)thiourea

Guidance literature:: In tetrahydrofuran; at 45 ℃; for 18h; chemoselective reaction;
DOI:10.1021/ja111480z

Reference yield:

: 1287225-51-7
(1S,2S,3R,4R,5S,6S)-2,3,4,5-tetrakis(benzyloxy)-6-(nonylamino)cyclohexanol

: 1287226-22-5
N-((3aR,4S,5R,6S,7S,7aS)-4,5,6,7-tetrakis(benzyloxy)-3-nonyl-hexahydrobenzo[d]oxazol-2(3H)-ylidene)nonan-1-amine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 18 h / 45 °C

2: mercury(II) oxide / toluene / 115 °C / Inert atmosphere

With mercury(II) oxide; In tetrahydrofuran; toluene;
DOI:10.1021/ja111480z