3-[3,5-bis(1-hydroxy-1-methylethyl)phenyl]-3-methylbutyl 2-bromo-2-methylpropionate

Base Information

Chemical Name:3-[3,5-bis(1-hydroxy-1-methylethyl)phenyl]-3-methylbutyl 2-bromo-2-methylpropionate
CAS No.:1383732-63-5
Molecular Formula:C₂₁H₃₃BrO₄
Molecular Weight:429.395
Hs Code.:

Synonyms:3-[3,5-bis(1-hydroxy-1-methylethyl)phenyl]-3-methylbutyl 2-bromo-2-methylpropionate

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Chemical Property of 3-[3,5-bis(1-hydroxy-1-methylethyl)phenyl]-3-methylbutyl 2-bromo-2-methylpropionate

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Technology Process of 3-[3,5-bis(1-hydroxy-1-methylethyl)phenyl]-3-methylbutyl 2-bromo-2-methylpropionate

There total 3 articles about 3-[3,5-bis(1-hydroxy-1-methylethyl)phenyl]-3-methylbutyl 2-bromo-2-methylpropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.1%

: 1246920-86-4
3-(3,5-diisopropylphenyl)-3-methylbutyl 2-bromo-2-methylpropionate

: 1383732-63-5
3-[3,5-bis(1-hydroxy-1-methylethyl)phenyl]-3-methylbutyl 2-bromo-2-methylpropionate

Guidance literature:: With N-hydroxyphthalimide; 4H₂O*Ac₂CoO₂; oxygen; In acetonitrile; at 23 ℃; for 72h;
DOI:10.1021/ma3007762

Reference yield:

: 763-32-6
2-methyl-1-buten-4-ol

: 1383732-63-5
3-[3,5-bis(1-hydroxy-1-methylethyl)phenyl]-3-methylbutyl 2-bromo-2-methylpropionate

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / tetrahydrofuran

2: aluminum (III) chloride / 25 h / -20 °C / Inert atmosphere

3: N-hydroxyphthalimide; 4H₂O*Ac₂CoO₂; oxygen / acetonitrile / 72 h / 23 °C

With aluminum (III) chloride; N-hydroxyphthalimide; 4H₂O*Ac₂CoO₂; oxygen; triethylamine; In tetrahydrofuran; acetonitrile; 2: Friedel Crafts alkylation;
DOI:10.1021/ma3007762

Reference yield:

: 1246920-85-3
3-methyl-3-butenyl 2-bromo-2-methylpropionate

: 1383732-63-5
3-[3,5-bis(1-hydroxy-1-methylethyl)phenyl]-3-methylbutyl 2-bromo-2-methylpropionate

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride / 25 h / -20 °C / Inert atmosphere

2: N-hydroxyphthalimide; 4H₂O*Ac₂CoO₂; oxygen / acetonitrile / 72 h / 23 °C

With aluminum (III) chloride; N-hydroxyphthalimide; 4H₂O*Ac₂CoO₂; oxygen; In acetonitrile; 1: Friedel Crafts alkylation;
DOI:10.1021/ma3007762