Diethyl-carbamic acid 2-[3-(2,2-dimethyl-propionylamino)-pyridin-4-yl]-phenyl ester

Base Information

Chemical Name:Diethyl-carbamic acid 2-[3-(2,2-dimethyl-propionylamino)-pyridin-4-yl]-phenyl ester
CAS No.:131653-67-3
Molecular Formula:C₂₁H₂₇N₃O₃
Molecular Weight:369.464
Hs Code.:

Synonyms:Diethyl-carbamic acid 2-[3-(2,2-dimethyl-propionylamino)-pyridin-4-yl]-phenyl ester

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Chemical Property of Diethyl-carbamic acid 2-[3-(2,2-dimethyl-propionylamino)-pyridin-4-yl]-phenyl ester

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Technology Process of Diethyl-carbamic acid 2-[3-(2,2-dimethyl-propionylamino)-pyridin-4-yl]-phenyl ester

There total 2 articles about Diethyl-carbamic acid 2-[3-(2,2-dimethyl-propionylamino)-pyridin-4-yl]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 113975-32-9
2,2-dimethyl-N-(4-iodo-3-pyridinyl)propanamide

: 103698-26-6
2,N,N,-diethylcarbamyloxyphenyl boronic acid

: 131653-67-3
Diethyl-carbamic acid 2-[3-(2,2-dimethyl-propionylamino)-pyridin-4-yl]-phenyl ester

Guidance literature:: With sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; for 12h; Heating;

Reference yield:

: 70298-88-3
N-(pyridin-3-yl)pivalamide

: 131653-67-3
Diethyl-carbamic acid 2-[3-(2,2-dimethyl-propionylamino)-pyridin-4-yl]-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1) BuLi, 2) I₂ / 1) Et₂O, -10 deg C, 2) -70 to -10 deg C

2: 87 percent / 2M aq. NaHCO₃ / Pd(PPh₃)4 / toluene / 12 h / Heating

With n-butyllithium; iodine; sodium hydrogencarbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene;